Agilent 1260 Infinity DAD and MWD User Manual 65
Using the Detector
4
Setting up an Analysis
Requirements and Conditions
Parts and Material required
Table 9 on page 65 lists the parts and material you need for the set up of the
analysis. Some of these are optional (not required for the basic system).
Conditions
A single injection of the isocratic test standard is made under the conditions
given in Table 10 on page 65:
Tabl e 9 Parts and Material required
Agilent 1260
Infinity system
Pump (plus degassing)
Autosampler
Detector, standard flow cell installed
• Agilent ChemStation or
• Instant Pilot G4208 (optional for basic operation) or
with with the appropriate revisions, see “Performance Specifications” on
page 24.
System should be correctly set up for LAN communication with the Data
System
Column: Zorbax Eclipse XDB C18, 150 mm x 4.6 mm, 5 µm (993967-906)
Standard: Agilent isocratic checkout sample (01080-68704). This 0.5 mL ampoule
contains 0.15 wt.% dimethylphthalate, 0.15 wt.% diethylphthalate, 0.01
wt.% biphenyl, 0.03 wt.% o-terphenyl in methanol.
Tabl e 1 0 Conditions
Flow 1.5 mL/min
Stoptime 8 minutes
Solvent 100 % (30 % water/70 % Acetonitrile)
Temperature Ambient
Wavelength sample 254 nm (4 nm bandwidth) reference 360 nm (100 nm bandwidth)
Injection Volume 1 µL
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