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Agilent 708-DS Dissolution Apparatus

Training Manual

Revision A September 2010

P/N: xx-xxxx

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AGILENT 708-DS DISSOLUTION APPARATUS

TRAINING MANUAL

Table of Contents

1.1. The Apparatus .......................................................................................................................... - 5 -

1.2. The Firmware ............................................................................................................................ - 6 -

1.3. Optional Configurations ........................................................................................................ - 6 -

2. INSTRUMENT SETUP ............................................................................. - 7 -

2.1. Physical Setup ......................................................................................................................... - 7 -

2.1.1. Unpacking Equipment / Accessories ....................................................................... - 7 -

2.1.2. Heater / Circulator Setup ............................................................................................. - 8 -

2.1.3. Communication / Power Cord Installation .............................................................. - 8 -

2.1.4. Instrument Power Up .................................................................................................... - 9 -

2.1.5. Leveling the Apparatus ................................................................................................ - 9 -

2.1.6. Heater / Circulator Power Up .................................................................................... - 10 -

2.1.7. Dissolution Vessel Installation ................................................................................. - 11 -

2.1.8. Manifold Installation .................................................................................................... - 11 -

2.1.9. Shaft / Evaporation Cover / DDM Installation ....................................................... - 12 -

2.1.10. Setting Paddle / Basket Heights .............................................................................. - 14 -

2.2. Firmware Setup – Instrument Settings ............................................................................ - 15 -

2.2.1. Apparatus ID Numbers, LCD Settings .................................................................... - 15 -

2.2.2. Setting the Date / Time ............................................................................................... - 16 -

2.2.3. Calibrating the Touch Screen ................................................................................... - 16 -

2.2.4. Instrument Tolerances, Vessel Size, Enable Alarms/DDMs ............................. - 17 -

2.2.5. Manifold Configuration (Vessel Numbering) ........................................................ - 17 -

2.2.6. Print Options ................................................................................................................. - 18 -

3. MEASUREMENT OF PHYSICAL PARAMETERS ................................. - 18 -

3.1. RPM, Wobble, Centering, Level, Verticality (Shaft and Vessel) ................................ - 18 -

3.1.1. RPM / Wobble................................................................................................................ - 19 -

3.1.2. Centering ....................................................................................................................... - 20 -

3.1.3. Vessel Table Level ....................................................................................................... - 20 -

3.1.4. Shaft / Vessel Verticality ............................................................................................ - 21 -

3.2. Temperature(s) ....................................................................................................................... - 21 -

3.2.1. External Vessel Temperature (EVT) Probe ............................................................ - 21 -

3.2.2. AutoTemp - Vessel Temperatures ........................................................................... - 22 -

3.3. Manual Operation (from Diagnostics) .............................................................................. - 23 -

3.3.1. Verification of Apparatus Operation ....................................................................... - 23 -

Agilent Technologies 708-DS Training Manual

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