33
Agilent 7697A Headspace Sampler
Troubleshooting
Agilent Technologies
4
Leaks
Leak Check General Procedure 34
Flow Paths 36
Checking for External Leaks 38
To Run the Restriction and Pressure Decay Test 40
To Run the Cross Port Leak Test 53
To Check for Leaks in the Transfer Line 58
This section discusses leak testing in the headspace sampler
(HS). Chromatographic symptoms such as loss of sensitivity
can result from leaks and restrictions. Use the following set
of tests for verifying leaks and restrictions within the HS.
Verify that the GC is leak free before checking for leaks
within the HS.