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G7166A
Agilent Technologies G7166A User Manual
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Agilent T
e
chnologies
Agilent InfinityLab LC Series
1260 Infinity II
Preparative Autosampler
User Manual
2
Table of Contents
Table of Contents
5
Default Chapter
9
Introduction
9
Product Description
10
1 Introduction
10
Features
11
Overview of the Module
12
Operating Principle
13
Sampling Sequence
13
Needle Parkstation
18
Hydraulic Box
19
Transport Assembly
21
Leak and Waste Handling
22
Leak Sensor
22
Waste Concept
23
2 Site Requirements and Specifications
25
Site Requirements
26
Physical Specifications
29
Performance Specifications
30
Specifications of the Sample Cooler
32
3 Using the Module
35
Magnets
36
Turn On/Off
37
Status Indicators
39
Exchange Drawers
40
Install the External Tray
42
Sample Trays
44
Choice of Vials and Caps
48
Transporting the Sampler with a Sample Cooler Installed
52
Agilent Local Control Modules
54
4 Installation of the Optional Sample Cooler
57
Injector Step Commands
58
Damaged Packaging
59
Install the Sample Cooler
60
Using the Sample Cooler in an Infinity II Sampler
65
Control Interface
66
Control
67
Temperature Mode
68
Online Signal Monitor
69
5 Preparing the Module
73
Leak and Waste Handling
74
Preparing the Module
75
Solvent Information
76
Capillary Color Coding Guide
82
Swage Fittings
83
Flow Connections to the Sampler
85
Setting up the Sampler
87
Control Settings
90
Method Parameter Settings
91
Injector Programm
95
Module Configuration View
96
6 Optimizing Performance
97
Optimization for Lowest Carry-Over
98
Using the Automated Needle Wash (Wash Port)
98
Using an Injector Program
100
General Recommendation to Lowest Carry-Over
101
Fast Injection Cycle and Low Delay Volume
102
Overlapped Injection Mode
102
General Recommendations for Fast Injection Cycle Times
103
Precise Injection Volume
104
Draw and Eject Speed
104
Choice of Rotor Seal
106
7 Troubleshooting and Diagnostics
107
Overview of the Module's Indicators and Test Functions
108
Maintenance Functions
110
User Interface
110
Change Needle
111
Change Metering Seal or Piston
113
Park Arm
114
Change Gripper
116
Automatic Referencing
117
Sampler Gripper Verification Test
118
Step Commands
119
Tests
120
Sample Cooler Function Test
120
Troubleshooting
121
Troubleshooting Guide for the Sample Transport Assembly
122
Intermittent Lock-Ups with or Without Vial in the Gripper Fingers
123
Poor Alignment
124
Agilent Lab Advisor Software
125
8 Error Information
127
What Are Error Messages
129
General Error Messages
130
Timeout
130
Shutdown
130
Remote Timeout
131
Lost CAN Partner
131
Leak Sensor
132
Leak Sensor Open
133
Leak Sensor Short
134
Compensation Sensor Open
134
Compensation Sensor Short
135
Fan Failed
135
Sampler Error Messages
136
Defective Gripper Assembly
136
Valve Failed
136
Needle Movement Failed
137
Missing Vial
137
Initialization Failed
138
Metering Home Failed
139
Motor Temperature
140
Initialization with Vial
141
Vial in Gripper
141
Missing Wash Vial
142
Invalid Vial Position
142
Valve Switch Not Found
143
Sample Cooler Error Messages
144
9 Maintenance
147
Introduction to Maintenance
148
Warnings and Cautions
149
Overview of Maintenance
151
Cleaning the Module
152
Remove and Install Doors
153
Exchange the Needle Assembly
154
Exchange the Needle Seat Assembly
159
Exchange the Sample Loop Assembly
164
Exchange the Rotor Seal
167
Exchange the Metering Seal and Piston
173
Exchange the Gripper Arm
177
Replace the Peristaltic Pump Cartridge
179
Exchange the Wash Port Assembly
182
Replace the Module Firmware
187
10 Parts and Materials for Maintenance
189
Main Assemblies
190
Standard Parts
191
Drawer Assembly
192
External Tray
194
Analytical-Head Assembly (900 Μl)
195
Standard Sampler Accessory Kit
196
Multi-Draw Kit
197
Additional Part List
198
11 Identifying Cables
199
Cable Overview
200
Analog Cables
202
Remote Cables
204
CAN/LAN Cables
208
RS-232 Cables
209
Usb
210
12 Hardware Information
211
Firmware Description
212
Electrical Connections
215
Rear View of the Module
216
Serial Number Information
216
Interfaces
217
Overview Interfaces
219
ERI (Enhanced Remote Interface)
221
USB (Universal Serial Bus)
224
Setting the 6-Bit Configuration Switch
225
Special Settings
227
Instrument Layout
229
Early Maintenance Feedback (EMF)
230
13 LAN Configuration
231
13 LAN Configuration What You Have to Do First
232
TCP/IP Parameter Configuration
233
Configuration Switches
234
Initialization Mode Selection
235
Dynamic Host Configuration Protocol (DHCP)
237
General Information (DHCP)
237
Setup (DHCP)
238
Manual Configuration
240
With Telnet
241
PC and Agilent Chemstation Setup
244
PC Setup for Local Configuration
244
Agilent Chemstation Setup
247
14 Appendix
253
General Safety Information
254
Safety Standards
254
General
254
Before Applying Power
255
Ground the Instrument
255
Do Not Modify the Instrument
256
Do Not Operate in an Explosive Atmosphere
256
Do Not Remove the Instrument Cover
256
Ground Solvent Lines
256
In Case of Damage
257
Solvents
258
Symbols
259
Waste Electrical and Electronic Equipment Directive
261
Refrigerant
262
Radio Interference
264
Sound Emission
265
Solvent Information
266
Agilent Technologies on Internet
267
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Agilent Technologies G7166A Specifications
General
Brand
Agilent Technologies
Model
G7166A
Category
Laboratory Equipment
Language
English
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