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AutoCAT 9000
Page 169 (Certification)
Hach AutoCAT 9000 - Certification; Product Safety and Immunity Standards; Emissions Standards
176 pages
Manual
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At Hach Company
, customer service is an
important part of every product we make.
W
ith that in mind, we have compiled the
following information for your convenience.
50081_GeneralInfoStop.fm
Page 167
General Information
168
170
Table of Contents
Main Page
Default Chapter
3
Table of Contents
3
Safety Information
7
Specifications
9
Introduction
11
General Information
11
Instrument Startup Summary
11
Unpacking
12
User Access Levels
13
Instrument Assembly
15
Instrument Assembly
17
Attaching the Titrant Bottle Holder
17
Connecting the Electrode Head and Accessories
17
Connecting the Titrant Bottle
18
Assembling the Burette
19
Connecting the Temperature Sensor
20
Installing the Electrode
21
Power Connection
21
Serial Printer and PC Connections
22
Operation
23
Basic Operation
25
Instrument Display and Keypad
25
Autocat Main Menus
26
How to Access the Menus
26
Methods Menu
26
Titrants Menu
27
Changing Titrants
27
Daily Start-Up
28
Electrodes Menu
28
Cell Menu
29
System Configuration
29
Entering the Supervisor Code
29
Setting a User ID
29
Choose a Language
29
Set the Time
30
Set the Date
30
Select Optional PC Keyboard
30
Selecting the Ac Power Frequency
30
Printer Status
31
Beep ON/OFF
31
Rules for Routine Access Users
31
Customizing the Station
32
Reset to Factory Settings
32
Exit
32
Edition Mode
32
Using Sub-ID's
33
Software Setup
35
Accessing Supervisor Mode
35
Software Setup for Electrode and Temperature Sensor Installation
36
Software Setup for Disconnecting or Replacing Electrodes
37
Software Setup for Burette Installation
38
Software Setup for Removing or Replacing the Burette
39
Software Setup for Titrant Installation
40
Software Setup for Switching or Replacing Titrants
41
Setting Titrant Concentration
42
Obtaining the Certificate of Analysis for Hach Reagents
43
Collecting and Accessing Data
45
Using the Autocat 9000 for Amperometric Methods
45
Autocat Titration
45
Data Collection
45
Current Range
45
Volume Increment
46
Predose Volume
46
Auto-Scaling
46
End Point Determination
46
Manual End Point Determination (MEPD)
47
Automatic End Point Determination (AEPD)
47
Auto Detection
47
Parameters Used in the Calculation of the Analyte Concentration
47
Titrant Concentration
47
Sample Volume
47
Dilution
48
Reductant Concentration
48
Reductant Volume
48
Analysis Calculations
48
Calculation of Mean
49
Calculation of Standard Deviation (<5 Replicate Analyses)
49
Retrieving Analysis Results from Archives
50
Calibration Procedures
51
PAO/5.64 Mn, Amperometric Forward Titrant Calibration
53
Iodine, Amperometric Back Titrant Calibration
59
Sampling
65
Chlorine
65
Container Pretreatment
65
Handling
65
Samples for Back Titration
65
Titration Procedures
67
Chlorine Dioxide
69
Generator Yield, Amperometric Forward Titration
69
Chlorine Dioxide, Amperometric Forward Titration
83
Free Chlorine, Amperometric Forward Titration
95
Total Chlorine, Amperometric Back Titration
101
Total Chlorine, Amperometric Forward Titration
107
Sulfite, Amperometric Back Titration
113
Total Oxidants, "Quick" Two Step Amperometric Titration
121
Chlorite, "Quick" Two Step Amperometric Titration
129
Manual Endpoint Determination
137
Below Detectable Limit
139
Maintenance
141
Instrument Maintenance
141
General
141
Display
141
Cleaning the Instrument
141
Cleaning and Conditioning the Electrode
141
Maintenance Intervals
142
Replacing the Fuse
142
Troubleshooting
143
Appendix A Amperometric Titration Theory
147
General Titration Theory
147
Redox Reactions
147
Reaction Measurement
147
Forward Vs. Back
147
Determining Concentration
148
Conversion Factor
148
Sample Spike
149
Errors and Interferences
149
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