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DOC-M88-EXX157_V17_04.2019 iii

Contents

1 Introduction.........................................................................................................................................5

1.1 Performance Verification Levels .........................................................................................6

1.2 Performance Verification in GxP Regulated Areas.............................................................7

2 Procedures..........................................................................................................................................9

2.1 Certified Reference Material ...............................................................................................9

2.2 Instrument Parameters .......................................................................................................9

2.3 Measurement Parameters ................................................................................................11

2.4 Evaluation Procedures and Data Interpretation................................................................12

2.4.1 Instruments with Primary Beam Monochromator..............................................................12

2.4.2 Instruments Without Focusing Monochromator ................................................................13

3 Reference Values..............................................................................................................................15

3.1 Angular Accuracy and Instrument Response....................................................................15

3.1.1 Basic Setup (Bragg-Brentano, dedicated and TWIN / TRIO Optics) ................................16

3.1.2 Additional Setups (Göbel Mirror, Parallel Beam TWIN / TRIO Optics) .............................16

3.1.3 Factory and Customer Acceptance Test Protocol ............................................................17

3.2 Instrument Resolution.......................................................................................................17

4 References – Glossary – Appendices A to I ..................................................................................19

4.1 References........................................................................................................................19

4.2 Glossary............................................................................................................................20

4.3 Appendices A to I..............................................................................................................20

A. Factory Acceptance Test Protocol.............................................................................................21

Declaration of Conformity .................................................................................................21

Bragg-Brentano Geometry with Copper Anode ................................................................21

Part I: Instrument Details (D8 Series) ...............................................................................23

Part II: Angular Accuracy, Instrument Response and Resolution (D8Series)..................29

B. Factory Acceptance Test Protocol.............................................................................................31

Declaration of Conformity .................................................................................................31

Bragg-Brentano Geometry with Cobalt Anode..................................................................31

Part I: Instrument Details (D8 Series) ...............................................................................33

Part II: Angular Accuracy, Instrument Response and Resolution (D8 Series)..................39

C. Factory Acceptance Test Protocol.............................................................................................41

Declaration of Conformity .................................................................................................41

Parallel Beam Geometry with Copper Anode ...................................................................41

Part I: Instrument Details ..................................................................................................43

Part II: Angular Accuracy, Instrument Response and Resolution.....................................47

D. Factory Acceptance Test Protocol.............................................................................................49

Declaration of Conformity .................................................................................................49

Parallel Beam Geometry with Cobalt Anode.....................................................................49

Part I: Instrument Details ..................................................................................................51

Part II: Angular Accuracy, Instrument Response and Resolution.....................................55

E. Customer Acceptance Test Protocol .........................................................................................57

Declaration of Conformity .................................................................................................57

Brand	Bruker
Model	D8 Series
Category	Laboratory Equipment
Language	English

Bruker D8 Series User Manual

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Bruker D8 Series Specifications

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