GE Sievers 500 RL - Page 100

GE Sievers 500 RL

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GE Analytical Instruments ©2010 100 of 226 DLM 74001-04 Rev. A

Chapter 4: Basic Analyzer Operation

Ambient Temperature Time Interval

Below 20 °C 15 minutes

20 - 30 °C 30 minutes

30 - 40 °C 90 minutes

Table of Contents

Identification Records2
- Table of Contents3
List of Tables9
List of Figures11
Revision History13
Trademarks and Patents14
Confidentiality15
Declaration of Conformity15
Standard Limited Warranty16
- Limitation of Remedies and Liability17
- Limitación de Remedios y Responsabilidad17
- Limites de Correction et de Fiabilité18
- Beschränkte Ansprüche und Haftung18
- Limitazione DI Rimedi E Responsabilità19
- 赔偿与责任限制20
Warnings21
Chapter 1: Introduction37
Chapter 2: System Description39
- System Specifications39
- System Overview41
- Sample Flow Path42
Analyzer Schematic (Shown with Standard Ios)42
- Additional System Components44
  - Microprocessor Controller and Electronics44
    - Data Outputs44
Chapter 3: Installation45
- Overview45
- Step 1: Unpack and Inspect the Analyzer46
  - Additional Installation Equipment47
- Step 2: Complete the Identification Records47
- Step 3: Select a Location for the Analyzer47
- Step 4: Install Power and Control Wiring48
  - Connecting to a Power Supply48
  - Installing the Analog Outputs and Alarms49
Wiring AC Power49
Alarm Outputs (TB2)50
- Table 3 Serial and 4-20 Ma Outputs (TB3)51
- Wiring the 4-20 Ma Connection51
Alarm Outputs (TB1)50
Filling the DI Water Cartridge57
Removing the John Guest Fitting58
- Step 8: Configure Basic Analyzer Settings59
- Step 9: Rinsing the Analyzer64
- Step 10: Install Datashare 500 Software65
Chapter 4: Basic Analyzer Operation67
- Overview67
  - The Main Screen67
- Figure 10 the Sievers 500 RL On-Line TOC Analyzer Main Screen68
- Setup69
  - Setting the Analyzer Mode69
  - Grab Mode Measurement Settings70
The Setup Tab70
- Taking TOC Measurements69
- The Menu Screen69
- Managing Data History71
  - Setting up Data History71
The Data Tab71
- Archiving Data History72
- Viewing Data History72
- Graphing Data History74
- Printing Data History75
- Exporting Data History76
- Setting up Analyzer Input and Output76
- Table 4 Data Fields Output to the Serial (RS-232) Port79
- Managing Maintenance Information85
- Advanced Analyzer Settings88
  - Exporting or Printing the Warning and Error History88
Figure83
Table83
Table84
- Figure 18 the Advanced Menu with One Program Language Loaded88
- Printing the Constants Values89
- Saving System Settings89
- Adjusting Display Contrast Settings90
- Changing the Display Mode90
- Naming the Analyzer Location90
- Specifying the Pharmacopeia91
  - Pharmacopeia Options91
  - Pass/Fail Reporting92
- Configuring the Flow Sensor93
- Selecting the Program Language93
- Programming the TOC Autozero94
- Specifying Auto Restart Settings94
- Activating Additional Features95
- Draining the Ios System95
- Basic Hardware Operation Issues96
The Super Ios System98
- Vial Set Cartridges99
- Steam Exposure99
- The Sample Inlet Block98
Chapter 5: Password Protection and Dataguard101
- Overview101
- Figure 22 Menu Map - Menu Lockout off (Requires Calibration Passwords)102
- Enabling Password Protection103
Menu Map - Dataguard (Optional Upgrade)103
- To Change the Password104
- To Configure Password Settings104
- To Enable Password Protection104
- Disabling Password Protection105
- Using Dataguard105
Audit Trail Output Format110
- Logging out111
Chapter 6: Calibration and System Protocols113
- Overview113
- Required Calibration Supplies114
- Preparing for Calibration115
- Disable Daily Download and Binary Input116
- Handling Standards116
- Perform Annual Maintenance Tasks116
- Performing a Single-Point Calibration117
Figure 29 the Accuracy, Precision, and Verification Summary Screen, Part 1126
Chapter 7: Maintenance139
- Replacing Consumables and Maintenance Items139
- Checking and Refilling the DI Water Level140
- Replacing the Sample Pump Tubing and Pump Heads144
- Replacing the DI Water Cartridge145
Table 15 Sievers 500 RL On-Line TOC Analyzer 3-Year Maintenance Worksheet151
Chapter 8: Troubleshooting153
- Overview153
- Step 1: Review Warnings and Errors153
  - Warnings and Error Messages154
- Step 2: Visual Inspection159
  - External Inspection159
  - Internal Inspection159
- Step 3: Review Solutions for Basic Problems159
  - The Analyzer will Not Power on160
  - No Flow through the Analyzer160
- Figure 40 Disconnecting the Tubing from the Front Solenoid Valve161
- Figure 41 the Inlet and Outlet Connections Inside the Analyzer162
- Negative, High, or Erratic Measurements163
- Problems Changing the Program Language165
- Problems with the DI Water Pump166
- Problems with Vial Set Cartridges166
- Step 4: Contact Technical Support167
- Step 5: Return the Analyzer to GE Analytical Instruments167
Figure 45 Analyzer Dimensions, with Standard Ios System171
Appendix A: Analyzer Dimension Diagrams171
Figure 46 Right-Side Analyzer Dimensions, with Standard Ios System172
Figure 48 Right-Side Analyzer Dimensions, with Super Ios System174
Figure 50 Right-Side Analyzer Dimensions, with Sample Inlet Block176
Appendix B: Connecting to a PC179
- Using Hyperterminal179
  - Determining Your Communications Port Number180
Index181

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