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Metrohm 756 KF User Manual
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7.2 Pin assignment of the "Remote" socket
756/831 KF Coulometer, Instructions for Use
132
7.2.2 Activate
pulse
An activate pulse may be set in key <PARAM>, >preselections, "activate pulse:". These
settings will be carried out as follows:
first cond.
all
inactive
START
Conditioning
START
Request id...
Start titration
end of det. (EOD)
Data output
139
141
Table of Contents
Default Chapter
5
Table of Contents
5
Introduction
9
Parts and Controls
10
The Wet Chemistry Workplace
12
Principle of Coulometric KF Determinations
12
Titration Vessel Setup
13
Your First Determination
14
Generator Electrode Without Diaphragm
15
Reagents
15
Cleaning
15
Generator Electrode with Diaphragm
16
Reagents
16
Cleaning
16
Tips for Working with Water Standards
17
Recommendations for Practise
17
Sample Addition
18
Sample Size
18
Liquid Samples
18
Solid Samples
18
Optimal Working Conditions
19
Drift
20
Reagent Exchange
21
Indicator Electrode
21
Manual Operation
22
Keypad
22
Principle of Data Input
23
Text Input
24
Configuration, Key <CONFIG
25
Reagent Exchange Procedure with Dosino
33
Mode Selection, Key <MODE
34
Parameters, Key <PARAM
35
Titration Sequence
39
Control Parameters and Ipol
40
Drift
40
Current at the Generator Electrode
41
Result Calculations
42
Statistics Calculations
45
Common Variables
47
Data Output
48
Reports for the Output at the End of a Determination
49
Additional Possibilities for Report Outputs
50
Display of the Titration Curve
50
User Name, Key <USER
51
Method Memory, Key <USER METH
52
Current Sample Data, Key <SMPL DATA
54
Silo Memory for Sample Data
55
Storing Determination Results and Silo Calculations
58
Storing Determination Results
58
Silo Calculations
59
Operation Via RS232 Interface
61
General Rules
61
Call up of Objects
62
Triggers
63
Status Messages
64
Error Messages
65
Remote Control Commands
68
Overview
68
Description of the Remote Control Commands
82
Properties of the RS 232 Interface
105
Handshake
105
Pin Assignment
108
Error Messages, Troubleshooting
111
Troubleshooting
111
Error and Special Messages
113
Initialize KF Coulometer
118
Testing the Measuring Input
119
Preparations
120
Coulometer Setup
120
Connecting a Stirrer or Ti Stand
120
Insert Paper into Built-In Thermal Printer
121
Titration Vessel Setup with Ti Stand
122
Connecting Coulometer to Dosino
123
Setup with Aspiration Equipment
123
Equipping the Titration Vessel for Aspiration
124
Connecting the KF Oven
125
Equipping the Titration Vessel with an Oven
126
Connecting the 774 Oven Sample Processor
127
Equipping the Titration Vessel with the Oven Sample Processor120
128
Connecting an External Printer
129
Connecting a Balance
130
Connecting a PC
131
Connecting a Remote Box
132
Connecting a Barcode Reader
132
Connecting a PC Keyboard
133
Appendix
135
Technical Specifications
135
Pin Assignment of the "Remote" Socket
137
Lines of Socket "Remote
139
Activate Pulse
140
Coulometer Validation, GLP Mode
141
Electronic Tests
141
Wet Tests
142
Maintenance and Adjustment of the Coulometer
142
User Methods
143
Working with the KF Oven
144
Working with the 774 Oven Sample Processor
146
Warranty and Certificates
148
Warranty
148
Certificate of Conformity and System Validation
149
KF Coulometer
149
EU Declaration of Conformity: 756 KF Coulometer
150
Certificate of Conformity and System Validation
151
KF Coulometer
151
EU Declaration of Conformity: 756 KF Coulometer
152
Scope of Delivery and Ordering Designations
153
Index
159
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Metrohm 756 KF Specifications
General
Brand
Metrohm
Model
756 KF
Category
Measuring Instruments
Language
English
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