Agilent InfinityLab LC Series RID User Manual 66
4 Preparing the Module
Setting up an Analysis
1
Open the purge valve of your pump (by turning it counterclockwise) and set
flow rate to 3–5mL/min.
2
Flush all tubes with at least 30 mL of solvent.
3
Set flow to required value of your application and close the purge valve.
Requirements and Conditions
What You Will Need
The table below lists the items you need to have for the set up of the analysis.
Some of these are optional (not required for the basic system).
Pump for approximately 10minutes before starting your application.
Do NOT exceed the flow rate of the 1290 Infinity II RID (Micro) whilst purging
pump. Bypass detector when purging >1mL/min.
Table 6 What you will need
Agilent 1200 Infinity Series system Pump (plus degassing)
Autosampler
Detector
Degasser (optional)
Column Compartment (optional)
Agilent CDS
System should be correctly set up for LAN communication
with the Agilent ChemStation
Column: Zorbax Eclipse XDB-C18, 4.6 x 150 mm, 5 µm (993967-902)
or an equivalent column
Standard: Agilent isocratic checkout sample (01080-68704)
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