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Agilent Technologies 5977C Series User Manual

Agilent Technologies 5977C Series
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Agilent 5977C Series GC/MSD
Operating Manual

Table of Contents

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Agilent Technologies 5977C Series Specifications

General IconGeneral
BrandAgilent Technologies
Model5977C Series
CategorySecurity Sensors
LanguageEnglish

Summary

Notices

Warranty Information

Details regarding the terms and conditions of the product warranty provided by Agilent.

Safety Notices Explained

Explanation of WARNING and CAUTION notices used throughout the manual for hazard identification.

1 Introduction

MSD Overview and Features

Describes the 5977C Series MSD versions, hardware components, and intended use of the instrument.

Safety Information

Covers important safety warnings, hydrogen safety, and regulatory certifications for the MSD.

Maintenance Procedures

Step-by-step guide on how to replace the primary fuses of the MSD.

2 Installing 8890 GC Columns

Column Installation and Conditioning

Covers column preparation, conditioning, tips, and installation into GC inlets and GC/MSD interfaces.

GC/MSD Interface Procedures

Details on installing the GC/MSD interface tip seal and the interface itself for 8890 GC systems.

3 Installing Intuvo 9000 GC Columns

Intuvo Column Handling and Installation

Guides on handling Intuvo GC columns, gaskets, guard chips, and tails for 9000 GC systems.

GC/MSD Interface Procedures

Instructions for installing the GC/MSD interface tip seal for Intuvo 9000 GC systems.

4 Operating in EI Mode

System Status and Configuration

Covers operating the MSD from the DS, WUI configuration, display readouts, and status LEDs.

Pre-Operation and Basic Procedures

Details on initial setup, including before turning on, pumping down, and venting the MSD.

Instrument Control and Monitoring

Managing temperatures, column flow, manual tune settings, and monitoring instrument parameters.

Tuning and Performance Verification

Procedures for tuning the MSD, verifying EI system performance, and performing high-mass testing.

JetClean System Operation

Setting the operation mode and parameters for the optional JetClean system.

5 Operating in CI Mode

CI Operation Fundamentals

General guidelines for CI operation, including autotuning and basic operation of the CI MSD.

CI System Setup and Configuration

Steps to set up software for CI, including methane and other reagent gas configurations.

Reagent Gas Control

Details on operating the reagent gas flow control module for CI analysis.

CI Performance Tuning and Verification

Procedures for PCI/NCI autotuning and verifying PCI/NCI performance.

Vacuum Monitoring

Instructions on how to monitor high vacuum pressure in CI mode.

6 General Maintenance

Safety and Precautions

Covers general safety, high voltage, temperatures, residue, and electrostatic discharge precautions.

Vacuum System Maintenance

Details on periodic maintenance tasks for the MSD vacuum system.

Analyzer Chamber Procedures

Guidance on maintaining the analyzer, including cleanliness and opening the chamber.

EI Source Maintenance

Procedures for removing, cleaning, assembling EI HES sources, and replacing filaments.

EI Source Handling and Replacement

Covers removing, disassembling, cleaning, and assembling various EI sources.

Filament and Electron Multiplier Replacement

Instructions for replacing filaments and the electron multiplier horn in EI sources.

7 CI Maintenance

CI Operation Setup and Guidelines

General information on CI operation, ion source cleaning, ammonia use, and setup guidelines.

Source Switching Procedures

Step-by-step guides for switching between EI and CI sources.

CI Source Radiator Procedures

Instructions for removing and installing CI source radiators.

CI Source Handling and Replacement

Procedures for removing, disassembling, cleaning, and assembling CI sources and filaments.

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