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G1314B
Agilent Technologies G1314B User Manual
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Agilent T
e
chnologies
Agilent 1260 Infinity
V
ariable W
avelength
Detector
User Manual
2
Table of Contents
Table of Contents
5
1 Introduction to the Variable Wavelength Detector
9
Introduction to the Detector
10
Optical System Overview
11
System Overview
16
2 Site Requirements and Specifications
19
Site Requirements
20
Physical Specifications
24
Performance Specifications
25
3 Installing the Detector
31
Unpacking the Detector
32
Delivery Checklist
33
Detector Accessory Kit Contents
33
Optimizing the Stack Configuration
34
One Stack Configuration
34
Two Stack Configuration
37
Installation Information on Leak and Waste Handling
39
Installing the Detector
43
Flow Connections to the Detector
46
4 Using the Detector
49
Leak and Waste Handling
50
Setting up an Analysis
51
Before Using the System
51
Requirements and Conditions
53
Optimization of the System
55
Preparing the HPLC System
56
Running the Sample and Verifying the Results
65
Special Settings of the Detector
66
Control Settings
66
Online Spectra
67
Scanning with the VWD
68
Analog Output Settings
69
Special Setpoints
70
5 How to Optimize the Detector
73
Optimizing the Detector Performance
74
Match the Flow Cell to the Column
75
Set the Detector Parameters
78
6 Troubleshooting and Diagnostics
79
Overview of the Detector's Indicators and Test Functions
80
Status Indicators
81
Power Supply Indicator
81
Module Status Indicator
82
Available Tests Versus Interfaces
83
Agilent Lab Advisor Software
84
7 Error Information
85
What Are Error Messages
86
General Error Messages
87
Timeout
87
Shutdown
88
Remote Timeout
88
Lost CAN Partner
89
Leak
90
Leak Sensor Open
90
Leak Sensor Short
91
Compensation Sensor Open
91
Compensation Sensor Short
92
Fan Failed
92
Open Cover
93
Detector Error Messages
94
UV Lamp: no Current
94
UV Lamp: no Voltage
94
Ignition Failed
95
No Heater Current
96
Wavelength Calibration Setting Failed
97
Wavelength Holmium Check Failed
98
Grating or Filter Motor Errors
98
Wavelength Test Failed
99
Cutoff Filter Doesn't Decrease the Light Intensity at 250 Nm
100
ADC Hardware Error
100
Cover Violation
101
8 Test Functions
103
Intensity Test
104
Intensity Test Failed
105
Cell Test
106
Wavelength Verification-Calibration
108
ASTM Drift and Noise Test
110
Quick Noise Test
111
Dark Current Test
112
Dark Current Test Failed
113
Holmium Oxide Test
114
Holmium Oxide Test Failed
116
9 Maintenance
117
Introduction to Maintenance
118
Warnings and Cautions
119
Overview of Maintenance
121
Cleaning the Module
122
Exchanging a Lamp
123
Exchanging a Flow Cell
126
Repairing the Flow Cells
128
Using the Cuvette Holder
130
Correcting Leaks
132
Replacing Leak Handling System Parts
133
Replacing the Interface Board
134
Replacing the Module's Firmware
135
10 Parts and Materials for Maintenance
137
Overview of Maintenance Parts
138
Standard Flow Cell 10 MM / 14 Μl
139
Micro Flow Cell, 5 MM / 1 Μl (Only for Support)
140
Micro Flow Cell 3 MM / 2 Μl
142
Semi-Micro Flow Cell 6 MM / 5 Μl
144
High Pressure Flow Cell 10 MM / 14 Μl
146
Cuvette Holder
148
Leak Parts
149
Kits
150
11 Identifying Cables
151
Cable Overview
152
Analog Cables
154
Remote Cables
156
BCD Cables
159
CAN/LAN Cables
161
RS-232 Cable Kit
162
External Contact Cable
163
12 Hardware Information
165
Firmware Description
166
Optional Interface Boards
169
Electrical Connections
172
Serial Number Information (ALL)
173
Rear View of the Module
174
Interfaces
175
Interfaces Overview
178
Setting the 8-Bit Configuration Switch (Without On-Board) LAN
182
Communication Settings for RS-232C
183
Special Settings
185
Instrument Layout
187
Early Maintenance Feedback (EMF)
188
EMF Counter
188
Using the EMF Counters
188
13 Appendix
191
General Safety Information
192
Batteries Information
195
Radio Interference
196
Sound Emission
197
UV Radiation
198
Solvent Information
199
Declaration of Conformity for HOX2 Filter
201
Agilent Technologies on Internet
202
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Agilent Technologies G1314B Specifications
General
Brand
Agilent Technologies
Model
G1314B
Category
Security Sensors
Language
English
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