Getting Started 
18  Agilent Cary 630 FTIR Spectrometer User’s Guide 
NOTE 
If the circle at the top of the software screen is yellow or red, contact Agilent 
technical support for assistance. 
Like any measurement device, it is important to verify that the Cary 
630 FTIR is performing properly before using the system to make 
critical measurements. The Cary 630 provides both diagnostic values 
and performance validation tests to demonstrate the system’s 
performance.  
The diagnostic values provide an easy to understand, quick 
assessment of the spectrometer’s function. If the spectrometer is not 
functioning properly, one of the diagnostic values will be out of 
specification. 
Performance validation tests are longer, more involved tests that 
measure how well the spectrometer is working. Validation tests check 
the spectrometer’s sensitivity (performance), stability and frequency 
precision (laser calibration).  
Each industry has different requirements for instrument verification. 
In general, the diagnostic values should be checked on a daily or 
weekly basis. Typically, the spectrometer will not collect data if the 
diagnostic values are grossly out of specification, but it is good 
practice to verify that the spectrometer is working properly.  
Performance validation should be run on a quarterly, bi-annual or 
annual basis. Highly-regulated industries may require the 
performance validation to be run monthly, depending on the use of 
the instrument.  
Diagnostic values 
The following values can be viewed on the Diagnostics page in the 
MicroLab PC software. In each case, the Optimal value indicates that 
the Cary 630 FTIR system is running at its intended performance 
level. The Marginal value indicates that the spectrometer is 
functioning, but at a lower performance level. The Critical value 
indicates that the system is not working correctly, in which case you 
should contact Agilent technical support for assistance.