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Bruker BioSpin minispec mq10 User Manual
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minispec
minispec mq-Series
User Manual
Version 001
Innovation with Integrity
●
AIC
2
Table of Contents
Table of Contents
3
1 About this Manual
5
Policy Statement
5
Symbols and Conventions
5
2 Safety
7
Intended Use
7
Qualified Personnel
7
Correct Usage
7
Electrical Safety
8
Lifting Safety
9
Personal Safety
9
Safety for Persons Wearing Pacemakers
9
Safety During Cryogen Refilling
10
Safety When Working with VT Probe Systems
11
Safety When Working with Glassware
11
3 Transport, Packaging and Storage
13
Symbols on the Packaging
13
Inspection at Delivery
14
Packaging
14
Storage
15
4 Technical Data
17
General Information
17
Connection Values
18
Operating Conditions
19
Rating Plate
20
Figure 4.1: the Minispec MQ-Series Rating Plate
20
5 Introduction
21
Figure 5.1: the Minispec Mq Magnet Unit (Left) and Electronic Control Unit (Right)
21
Improvements
22
Siting Considerations
22
Environmental Considerations
23
Installation of the Minispec Mq-Series
24
Unpacking the System
25
Figure 5.2: the Minispec Magnet Unit (Left) and Electronic Control Unit (Right)
25
Figure 5.3: Handles on the Side of the Magnet Unit
26
Electronic Control and the Magnet Unit Connections
27
Figure 5.4: Electronic Control and Magnet Units
27
Figure 5.5: Back Planes of the Electronic Control Unit (Top) and Magnet Unit (Bottom)
27
Electronic Control, Magnet and Gradient Unit Connections
28
Figure 5.6: Sketch of the Back View of the Connections from the Gradient Unit
28
Figure 5.7: Back View of the Gradient Unit
28
Specifications Mq-Series
29
Weights and Dimensions
29
Electrical Specifications
29
Interpretation of the Leds
30
Mq-Series Systems
30
Calibration Samples Hatch and Probe Exchange
31
Figure 5.8: Ring of the Quick-Release Fastener (Left) and the Raising of the Probe Assembly (Right)
31
6 Getting Started
33
Software Installation
33
Connecting the PC to the Minispec for the First Time
34
Direct Cable Connection
34
Connection to a Network
35
Wake-Up State of the Minispec.exe Software
35
Configuration of the Software, the Welcome Box
35
Figure 6.1: the Welcome Box
35
Selecting Applications and Connections
36
Changing Analyser Type and Calibration Permission
36
General Measurement Handling
36
List of Standard Applications
37
7 The Minispec Standard Windows
39
The Signal Window
39
The Results Window
39
Figure 7.1: the View of the Signal Window, Result Window and the Spread Sheet
39
The Spreadsheet Window
40
Execution of Spreadsheets
40
Saving Spreadsheets
40
Monitoring
40
8 The Minispec Menu Functions
41
The Bars
41
The File Menu
42
Figure 8.1: the Default View
42
Figure 8.2: the File Pull-Down Menu
42
Figure 8.3: the Dialog Box for Data Saving Setup
44
The Edit Menu
45
Figure 8.4: the Edit Pull-Down Menus for Different Active Windows
45
The Minispec Menu
46
Figure 8.5: the Minispec Pull-Down Menu
46
Figure 8.6: the Minispec Settings Table
47
The Measurement Menu
49
Figure 8.7: the Measurement Pull-Down Menu
49
The Parameter Menu
51
The Acquisition Parameter Table Command
51
Figure 8.8: the Parameter Pull-Down Menu
51
Figure 8.9: the Acquisition Parameter Table
52
The Application Configuration Table Command
53
The Acquisition Pre-Delay Time Command
54
The Repetitive Measurement Settings Command
54
The View Menu
54
Figure 8.10: the View Pull-Down Menu
54
Figure 8.11: the Statistics Box
56
Figure 8.12: Display Modes
56
The Process Menu
58
Figure 8.13: the Process Pull-Down Menu
58
The Window Menu
59
Figure 8.14: the Window Pull-Down Menu
59
The Help Menu
60
Figure 8.15: the Help Pull-Down Menu
60
9 The Experiment Editor Expspel for the Mq-Series
61
10 Basic NMR Principles
63
Figure 10.1: Increase of the NMR Signal Due to Longitudinal Relaxation
63
Figure 10.2: Decay of the NMR Signal Due to Transverse Relaxation
64
11 Maintenance
65
Cleaning
65
12 Dismantling and Disposal
67
Dismantling
67
Disposal
67
13 Contact
69
List of Figures List of Figures
71
List of Figures
71
Index
73
4
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Bruker BioSpin minispec mq10 Specifications
General
Brand
Bruker BioSpin
Model
minispec mq10
Category
Measuring Instruments
Language
English
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