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Micromeritics TriStar II 3020 - Page 60

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6 Installation Checklists
Procedure
Evaluation
Code
Initial /
Date
Create sample files for nitrogen analysis.
P F N/A
Create additional sample files for krypton analysis, if applicable.
P F N/A
Clean sample tubes P F N/A
Determine sample mass.
P F N/A
Degas samples.
Install sample tubes.
Prepare the dewar.
Perform blank tube run. Blank tube run must be within tolerances:
l 3/8 in. less than ± 0.073 STP cm
3
at any point
l 1/2 in. tube less than ± 0.200 STP cm
3
at any point
Perform carbon black reference material analysis with nitrogen gas.
Use table below to record results.
Reference Material Analysis
Port 1:Carbon Black
Initial / Date
Expected BETresults:_______________±_______________
Actual BETresults: ________________±________________
Y N N/A
Port 2:Carbon Black
Initial / Date
Expected BETresults:_______________±_______________
Actual BETresults: ________________±________________
Y N N/A
Port 3:Carbon Black
Initial / Date
Expected BETresults:_______________±_______________
Actual BETresults: ________________±________________
Y N N/A
6 - 6
TriStar II 3020 Confirm Installation Instructions and Checklist
302-42870-04 (Rev A) Sep 2017

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