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Micromeritics TriStar II 3020 - Step 1 - Clean and Label Sample Tubes

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STEP 1 - CLEAN AND LABEL SAMPLE TUBES
Sample tubes and filler rods must be clean and dry before samples are added and weighed. The
following table indicates which materials are supplied by Micromeritics and which are supplied by the
user. The procedures following the materials table are recommended.
Supplied by Micromeritics
Supplied by User
l Filler rod
l Sample data worksheet
l Sample tube
l Sample tube brush
l Sample tube rack
l Sample weighing support
l Stopper for sample tube
l Acetone or isopropyl alcohol
l Analytical balance
l Detergent
l Drying oven
l Pipe cleaners
l Rubber gloves or lint-free cloth
l Safety glasses
l Ultrasonic cleaning unit
l Waste container
1. Preheat drying oven to 110 ºC.
2. Verify that the ultrasonic cleaning unit is clean.
3. Use 5 grams of Alconox (or other suitable detergent) per 500 ml of warm water and fill the
ultrasonic unit with enough water to cover the sample tubes and filler rods (if used). If too
much detergent is used, it may be difficult to rinse from the sample tubes. Ensure the deter-
gent is dissolved before placing the sample tubes and filler rods into the water.
4. Fill the sample tubes with warm water and place them in the ultrasonic cleaning unit, then
place the filler rods in the unit. Turn on the ultrasonic cleaning unit for approximately fifteen
minutes.
Step 1 - Clean and Label Sample Tubes
TriStar II 3020 Confirm Installation Instructions and Checklist
302-42870-04 (Rev A) Sep 2017
5 - 7

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