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TRISTAR II PLUS
Micromeritics TRISTAR II PLUS User Manual
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O
PERATOR
M
ANUAL
303-42800-01
Sep
2023
(Rev
M
)
T
RI
S
TAR
®
II
P
LUS
S
URFACE
A
REA
AND
P
OROSITY
A
NALYZER
2
Table of Contents
About this Manual
6
General Safety
7
Table of Contents
11
1 Analyzer Components for Tristar II Plus
17
Equipment Options and Upgrades
20
Gas Requirements and Purity
22
Cryogen Requirements
22
Specifications for the Tristar II Plus
23
2 About the Software
27
Menu Structure
28
Common Fields and Buttons
29
File Status, Description, and Location
32
Keyboard Shortcuts
34
Option Presentation
36
Libraries
38
Methods
39
Configure the Analyzer
41
Specify Gas Ports and Unit Configuration
41
Unit Selection
42
Instrument Status
43
Show Dashboard
43
Show Instrument Log
45
Show Instrument Schematic
47
Show Status
48
Convert Files
48
Export Files
49
List Files
50
Software Uninstall
51
Software Updates
51
Software in 21CFR11 Environments
53
Uninstall Software in 21CFR11 Environments
56
3 Sample Files
57
Create Sample Files
58
Open a Sample File
61
Manually Enter Data
63
4 Parameter Files
69
Adsorptive Properties
70
Analysis Conditions
73
Degas Conditions
81
Report Options
84
Sample Tube
86
5 Degassing
89
Degas on the Smart Vacprep
89
Transfer a Degassed Sample to an Analysis Port
89
6 Perform an Analysis
93
Dewar Precautions
93
For Glass Dewars
94
Prepare for Analysis
95
Clean and Label Sample Tubes
95
Create the Sample File
97
Determine the Sample Mass
97
Degas the Sample
99
Sample Tube Installation
100
Fill and Install the Dewar
103
Perform a Krypton Analysis
105
Perform a Quickstart Analysis
107
Perform a Sample Analysis
109
Perform a Sample Tube Free Space Analysis
113
Perform an Empty Tube Analysis
115
Perform a Reference Material Analysis
116
7 About Reports
117
Start Reports
117
Heat of Adsorption Report
118
SPC Report
120
Regression Report
121
Control Chart Report
123
Microactive Reports
126
Interactive Reports
127
Evaluate Report Results
128
Report Features and Shortcuts
134
Graph Features and Shortcuts
139
Graph and Sample Overlays
143
Generate Pore Size Distribution Graph Overlays
144
Overlay Multiple Sample Files
147
Import ASCII Pore Distribution Data
150
Report Examples
151
BET Report
151
BET Surface Area Plot
152
BJH Adsorptive Cumulative Pore Volume
153
BJH Desorption Cumulative Pore Volume
154
Isotherm Linear Plot
155
Isotherm Log Report
156
T-Plot
157
8 Selected Report Options
159
Advanced Reports - Python Module
159
Alpha-S Method Report
162
BET Surface Area Report
164
BJH Adsorption/Desorption Report
166
DFT Pore Size Report
172
DFT Surface Energy Report
175
Dollimore-Heal Adsorption/Desorption Report
176
Dubinin Report
180
F-Ratio Method Report
185
Freundlich Report
187
Horvath-Kawazoe Report
189
Isotherm Report
193
Langmuir Report
195
MP-Method Report
197
NLDFT Advanced PSD Report
201
Options Report
205
Sample Audit Trail Report
206
Summary Report
207
T-Plot Report
209
Temkin Report
212
Validation Report
214
9 Diagnostics
215
Show All Readings
215
Start Diagnostic Test
215
10 Calibration
217
Match Transducers
218
Pressure Offset
219
Servo Valve
220
Save Calibration to File
220
Load Calibration from File
221
11 Troubleshooting
223
Power
225
Guidelines for Connecting Gases
226
Replace a Gas Cylinder
227
Clean and Verify the Gas Line
231
Enable Manual Control
233
Perform a Leak Test
234
Preventive Maintenance
236
Check and Clean the Dewar
237
Clean the Instrument
238
Clean the Gas Delivery Tubes
238
Lubricate the Elevator Drive Assembly
238
Power Instrument on and off
239
Sample Port Frit Replacement
240
Sample Tube O-Ring Replacement
241
Recover from a Power Failure
242
Service Test Mode
243
Oil-Based Vacuum Pump
243
Parts and Accessories
243
Advanced Reports a
246
Scripts a
248
Python Reports a
250
Acquire Basic Information a
254
Acquire Report Results a
256
Acquire Overlay Sample Data a
258
Enable the Use of Overlay Data a
260
B DFT Models
275
Models Based on Statistical Thermodynamics B
275
Models Based on Classical Theories B
287
DFT Model References B
290
C Free-Space Correction
293
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Micromeritics TRISTAR II PLUS Specifications
General
Brand
Micromeritics
Model
TRISTAR II PLUS
Category
Measuring Instruments
Language
English
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