42 Purification Solution - Developer's Guide
4
Setting Up and Running a Purification Task
Reviewing analytical results
Reviewing analytical results
1 If you have selected to review the analytical results before starting the
preparative run, the purification run stops after the evaluation of the
analytical results. Select the Analytical Results tab to review the results.
You can make any adjustments to the scale-up parameters and preparative
run conditions before continuing with the purification step.
In the Analytical Results tab, the identified target compound and the
calculated gradient profile are visualized. Spectral data of each peak is
displayed in the Spectra tab. Scale-up, integration and fraction collector
thresholds can be adjusted for each sample individually. Target masses or
formulas can be corrected.
2 When you are satisfied with the results, click Run in the top toolbar of
the Ta sk dialog box to start the preparative run.
3 When the preparative run is finished, select the Preparative Results tab to
review the results.
All changes in the Analytical Results tab apply to the selected sample, so you must step
through all samples that you want to review or for which you want to change settings. If
settings have to be adjusted for all samples, return to the Task Configuration tab to
change the global settings, then restart the evaluation of the analytical results.
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