4 Purification Solution - Developer's Guide
Contents
Contents
1 The Role of the Method Developer 7
2 Preparing Default Purification Methods 9
General Method Settings 11
Analytical Method Settings 16
Preparative Method Settings 19
Agilent Active Splitter (G1968D/E/F) 23
Critical Method Parameters 24
3 Setting Up an Analytical and Preparative System 27
Setting up an analytical system 28
Setting up a preparative system 30
4 Setting Up and Running a Purification Task 33
Setting up a purification task 34
Configuring a new task 35
System Suitability Tests 38
Running a task 39
Processing partial data and cloning tasks 40
Reviewing analytical results 42
5 Reviewing Purification Results 43
6 Calibration Procedures 45
Characterizing the delay volumes: Mixing point to UV detector and Column to UV
detector 48
Characterizing the column volume 63
System Configuration and Delay Time Calibration 70
7 Checkout Procedure 83
Acquire an analytical run using the Chemstation sequence 85
UV-only Workflow: Focused gradient in the Purification software 89
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