EasyManua.ls Logo

Agilent Technologies 1290 - User Manual

Agilent Technologies 1290
302 pages
Print Icon
To Next Page IconTo Next Page
To Next Page IconTo Next Page
Loading...
Agilent Technologies
Agilent 1290 Infinity
Quaternary Pump
User Manual

Table of Contents

Other manuals for Agilent Technologies 1290

Question and Answer IconNeed help?

Do you have a question about the Agilent Technologies 1290 and is the answer not in the manual?

Agilent Technologies 1290 Specifications

General IconGeneral
BrandAgilent Technologies
Model1290
CategoryLaboratory Equipment
LanguageEnglish

Summary

Notices

Warranty

Details the warranty terms for the manual's content, disclaiming liability for errors.

Technology Licenses

Describes terms for hardware and software use, furnished under license.

Restricted Rights Legend

Outlines rights for U.S. Government use of software, subject to standard license terms.

Safety Notices

Explains CAUTION and WARNING notices for hazards and precautions.

Introduction

Features

Details the key features of the G4204A Quaternary Pump for high performance.

Overview of the Quaternary Pump

Provides a general description of the pump's capabilities and applications.

Operating Principle

Explains how the pump operates mechanically and electronically.

Positions of the Multi Purpose Valve

Illustrates valve positions in different operating modes like Purge and Filter Flush.

System Overview

Highlights leak and waste handling concepts within the system.

Site Requirements and Specifications

Site Requirements

Details environmental and operational requirements for optimal instrument performance.

Power Considerations

Discusses power supply capabilities, safety precautions for voltage and grounding.

Power Cords

Explains power cord options and critical safety warnings for use.

Bench Space

Specifies required space for module placement and air circulation.

Condensation

Warns about condensation and its potential to damage system electronics.

Physical Specifications

Lists physical dimensions, weight, voltage, frequency, and temperature ranges.

Performance Specifications

Details hydraulic system, flow, pressure, and composition specifications.

Installing the Module

Unpacking the Module

Instructions for handling damaged packaging and checking delivery.

Delivery Checklist

Ensures all parts and materials are delivered with the module.

Optimizing the Stack Configuration

Guides on configuring modules for optimum performance and minimum delay volume.

One Stack Configuration

Recommended setup for a single stack of modules for minimum delay volume.

Two Stack Configuration

Recommended setup for a two-stack system to avoid high stacks.

Installation Information on Leak and Waste Handling

Details safe leak and waste handling procedures and precautions.

Removing the Transport Foam

Step-by-step guide to carefully remove protective foam from the module.

Installing the Pump

Procedure for placing the module on a bench and ensuring power is off.

Flow Connections to the Pump

Describes the installation of additional flow connections to the pump.

Installation of Seal Wash Option

Instructions for installing the optional seal wash function.

Using the Pump

Leak and Waste Handling

Guidelines for safe handling of leaks and waste, including solvent precautions.

Preparing the Pump

Steps to prepare the pump for optimal performance, including solvent and filter checks.

Algae Growth in HPLC Systems

Explains causes, problems, and prevention of algae growth in HPLC systems.

Setting up the Pump with the Instrument Control Interface

Guides on configuring the pump via the instrument control interface.

The Pump User Interface (Dashboard Panel)

Explains items and functions in the pump graphic interface.

Instrument Signals

Lists and describes the pump signals displayed, such as Flow and Pressure.

Context Menu

Details commands available in the dashboard context menu for pump control.

Control Settings

Describes pump control parameters like Pump, Seal Wash, Purge, and Prime.

Method Parameter Settings

Details pump method setup parameters like Flow, Solvents, Timetable, and Blend Assist.

Advanced Settings

Covers advanced method setup parameters like Minimum Stroke and Compressibility.

Timetable Settings

Programs parameter changes during analysis via timetable entries.

Blend Assist

Allows blending solvents or solvent mixtures from stock solutions.

Priming the Pump

Instructions for priming the pump system with solvent after exchanges or downtime.

Flushing the Filter

Procedure for flushing the inline and outlet filters.

Solvent Information

Recommendations on solvent use and materials in the flow path for compatibility.

How to Optimize the Performance of Your Module

Using the Degasser

Explains the importance and use of the built-in degasser for flow path stability.

Operational Hints for the Multi Channel Gradient Valve (MCGV)

Provides hints for using the MCGV with salt and organic solvents to prevent precipitation.

Delay Volume and Extra-Column Volume

Defines and explains system volume effects on chromatography and gradient shape.

How to Configure the Optimum Delay Volume

Guides on configuring delay volume and using the optional Jet Weaver mixer.

How to Achieve Higher Resolution

Explains how to increase separation resolution by optimizing selectivity, particle size, and columns.

Using Solvent Calibration Tables

Details importing solvent calibration data for optimum pump control and accuracy.

Troubleshooting and Diagnostics

Overview of the Module’s Indicators and Test Functions

Explains status indicators, error messages, test functions, and diagnostic signals.

Status Indicators

Location and meaning of front module status indicators: power and module status.

Power Supply Indicator

Indicates power status via an illuminated green light on the power switch.

Module Status Indicator

Describes conditions indicated by the module status LED: OFF, Green, Yellow, Red, Blinking.

Available Tests vs User Interfaces

Compares available tests across different user interfaces, recommending Agilent Lab Advisor.

Agilent Lab Advisor Software

Details the Agilent Lab Advisor software features, versions, and add-ons.

Error Information

What Are Error Messages

Explains how error messages are displayed, propagated, and resolved.

General Error Messages

Lists generic error messages applicable to HPLC modules like Timeout and Shutdown.

Timeout

Error ID 0062: Timeout threshold was exceeded, indicating a potential not-ready condition.

Shutdown

Error ID 0063: External instrument generated shutdown signal via remote connector.

Remote Timeout

Error ID 0070: Not-ready condition persists on the remote input line.

Lost CAN Partner

Error ID 0071: Failed synchronization or communication between modules in the system.

Leak Sensor Short

Error ID 0082: Leak sensor failed due to a short circuit.

Leak Sensor Open

Error ID 0083: Leak sensor failed due to an open circuit.

Compensation Sensor Open

Error ID 0081: Ambient compensation sensor failed (open circuit).

Compensation Sensor Short

Error ID 0080: Ambient compensation sensor failed (open circuit).

Fan Failed

Error ID 0068: The cooling fan in the module has failed.

Leak

Error ID 0064: A leak was detected in the module, causing system shutdown.

Pump Error Messages

Lists pump-specific errors like pressure limits, solvent counters, and drive issues.

Pressure of quaternary pump above upper limit

Error ID 29163: Pressure exceeded the upper pressure limit.

Pressure below lower limit

Error ID 29176: Pressure dropped below the lower limit.

Target pressure not reached for quaternary pump degasser

Error ID 29221: Degasser target pressure not reached within the expected time.

Solvent counter exceeded limit

Error ID 29146: Solvent volume counter exceeded the set limit.

Waste counter limit exceeded

Error ID 29147: Waste volume counter exceeded the set limit.

Flow rate limit exceeded

Error ID 29164: Flow rate exceeded limit while pump is in pressure control.

Quaternary pump shutdown during analysis

Error ID 29199: Pump shut down by control software during an analysis.

Reading the pump encoder tag failed

Error ID 29201: Failed to read the pump encoder tag.

Writing the pump encoder tag failed

Error ID 29200: Failed to write the pump encoder tag.

Pump drive blocked or encoder failed

Error ID 29214: Pump drive is blocked or encoder has failed.

Drive current too low

Error ID 29205: Pump drive current consumption is too low.

Drive current too high

Error ID 29236: Pump drive current consumption is too high.

Drive timeout

Error ID 29204: Drive movement blocked mechanically during initialization.

Overcurrent of pump drive

Error ID 29202: Pump drive current consumption is too high.

Deliver underrun

Error ID 29233: Internal error related to delivery underrun.

Defect connection between main board and pump drive encoder

Error ID 29208: Defect connection between main board and pump drive encoder.

Pump drive encoder defect

Error ID 29209: Defect identified in the pump drive encoder.

Multi Purpose Valve failed

Error ID 29231: Lost steps detected in the purge valve encoder.

Reading of multi purpose valve tag failed

Error ID 29240: Failed to read the multi purpose valve tag.

Pump drive encoder rollover

Error ID 29232: Invalid pump drive encoder signals detected.

Drive position limit

Error ID 29234: Internal error related to the drive position limit.

Insufficient power of drive encoder LED

Error ID 29235: Insufficient power detected for the drive encoder LED.

Drive encoder error

Error ID 29237, 29238, 29239, 29215: General pump drive encoder error.

Writing the multi purpose valve tag failed

Error ID 29241: Failed to write the multi purpose valve tag.

Unknown multi purpose valve type

Error ID 29242: Invalid type information detected for the multi purpose valve.

Pump drive encoder error

Error ID 29211: Pump drive encoder generated no signal.

Pump drive error

Error ID 29212, 29213: Pump drive failed during calibration.

Maximum stroke is too short

Error ID 29203: The maximum stroke detected is too short.

Pump drive stop not found

Error ID 29207: The pump drive stop position was not found.

Timeout: Wait for Composition

Error ID 29180: Target composition not reached within the expected time frame.

Timeout: Wait for run volume

Error ID 29181: Target run volume not reached within the expected time frame.

Timeout: Wait for Volume

Error ID 29182: Target volume not reached within the expected time frame.

Timeout: Wait for Flow

Error ID 29183: Target flow rate not reached within the expected time frame.

Timeout: Wait for Pressure

Error ID 29185: Target pressure not reached within the expected time frame.

Drive Encoder failed

Error ID 29210: Drive encoder failed during pump drive calibration.

Drive phases differ too much in electric resistance

Error ID 29216: Calibration failed due to electric resistance differences.

Degassers pressure limit violation

Error ID 29220: Degasser pressure is too far above the specified limit.

Seal wash pump was missing when tried to turn on

Error ID 29223: Seal wash pump not detected during configuration.

Valve hardware overcurrent (MCGV)

Error ID 29227: Power consumption too high for one of the MCGV valves.

Test Functions and Calibrations

Maintenance

Introduction to Maintenance

Shows user-accessible assemblies for simple repairs without removing the pump.

Warnings and Cautions

Details safety warnings for solvents, electrical shock, and product use.

Overview of Maintenance

Describes maintenance procedures that can be done without opening the main cover.

Cleaning the Module

Instructions for cleaning the module case with a soft cloth and mild detergent.

Installing Fittings and Capillaries

Steps for installing and properly tightening fittings and capillaries.

Replacing the Pressure Sensor

Procedure to replace the pressure sensor when no or invalid pressure signal is detected.

Replacing the Inlet Weaver

Step-by-step guide to replace the inlet weaver assembly.

Replacing the Inlet Valve

Procedure for replacing a defective inlet valve using a torque wrench.

Replacing the Outlet Valve

Instructions for replacing a defective outlet valve, including seal replacement.

Removing the Jet Weaver

Steps to remove the Jet Weaver from the front panel.

Installing the Jet Weaver

Procedure for installing the optional Jet Weaver mixer for improved mixing performance.

Replacing the Seal Wash Pump

Instructions for replacing the seal wash pump when it shows signs of wear.

Replacing the Multi-Channel Gradient Valve (MCGV)

Step-by-step guide to replace the Multi-Channel Gradient Valve (MCGV).

Releasing a Stuck Inlet Valve

Procedure to release a stuck inlet valve using a syringe and wash solvent.

Replacing the Pump Head

Procedure for replacing the pump head assembly for maintenance or performance issues.

Disassembling the Pump Head

Steps for disassembling the pump head assembly, recommending refurbished parts.

Disassembling the Primary Pump Head

Detailed steps for disassembling the primary pump head, with piston cautions.

Disassembling the Secondary Pump Head

Detailed steps for disassembling the secondary pump head, with piston cautions.

Replacing the Heat Exchanger

Instructions for replacing the heat exchanger, noting it's not needed for pump head maintenance.

Replacing Wash Seal and Gasket

Procedure for replacing the wash seal and gasket using an insert tool.

Assembling the Pump Head

Steps for assembling the pump head using alignment tools and torque specifications.

Parts and Materials

Overview of Main Assemblies

Illustrates and lists main maintenance parts with item numbers and p/n.

Flow Connections

Diagrams and descriptions of pump flow connections with item numbers.

Seal Wash Option

Details the peristaltic pump and tubing for the optional seal wash function.

Pump Head Assembly Parts

Lists and illustrates parts for pump head assemblies with item numbers and p/n.

Primary Pump Head Parts

Details primary pump head components with and without seal wash.

Secondary Pump Head Parts

Details secondary pump head components with and without seal wash.

Multi Purpose Valve

Illustrates and lists parts for the multi-purpose valve with item numbers and p/n.

Solvent Cabinet

Illustrates and lists parts for the solvent cabinet with item numbers and p/n.

Cover Parts

Illustrates and lists parts for the pump module covers with item numbers and p/n.

Leak Parts

Illustrates and lists parts related to leak detection and handling.

Accessory Kit

Lists items included in the Accessory Kit for the 1290 Infinity Quaternary Pump.

HPLC System Tool Kit

Lists accessories and tools needed for installation and repair of the module.

1290 Infinity Pump Service Kit

Lists components included in the 1290 Infinity Pump Service Kit.

Identifying Cables

Cable Overview

Provides an overview of available cable types: Analog, Remote, BCD, CAN/LAN, RS-232.

Analog cables

Details analog cables and their BNC connector pin assignments.

Remote Cables

Describes remote cables for Agilent integrators and A/D converters.

BCD Cables

Details BCD cables and their pin assignments for general purpose and integrators.

CAN;LAN Cable

Describes CAN and LAN cables with modular plugs for module connections.

RS-232 Cable Kit

Details RS-232 cable specifications, pin-out, and compatibility.

Agilent 1200 Module to Printer

Describes cable for connecting Agilent 1200 modules to printers via Serial/Parallel.

Hardware Information

Firmware Description

Explains the instrument firmware structure: resident and main system sections.

Firmware Updates

Details tools and procedures for updating instrument firmware.

Electrical Connections

Explains CAN, REMOTE, RS-232C, and power input connections and safety.

Rear View of the Module

Diagram showing rear panel connectors, switches, and labels.

Interfaces

Lists interfaces (CAN, LAN, RS-232, Analog, APG) for Agilent 1200 Infinity Series modules.

Overview Interfaces

Details CAN, LAN, and RS-232C interface functionalities and pin definitions.

Setting the 8-bit Configuration Switch

Explains configuration switch settings for LAN, RS-232, and initialization modes.

Special Settings

Describes Boot-Resident and Forced Cold Start modes for specific actions.

Early Maintenance Feedback

Explains EMF for monitoring component usage and scheduling maintenance.

Instrument Layout

Describes the module's industrial design and packaging technology.

LAN Configuration

What You Have To Do First

Notes MAC address and connects instrument LAN interface to PC.

TCP;IP Parameter Configuration

Explains IP address, Subnet Mask, and Gateway configuration methods.

Configuration Switch

Location and default settings of the rear panel configuration switch.

Initialization Mode Selection

Describes selectable initialization modes: Bootp, Stored, Default, DHCP.

Dynamic Host Configuration Protocol (DHCP)

Explains DHCP for automatic IP address assignment on HPLC modules.

Setup (DHCP)

Steps to set up DHCP initialization mode using configuration switches.

Link Configuration Selection

Manually sets link operating mode for non-auto-negotiating network devices.

Automatic configuration with Bootp

Details the Agilent BootP Service for assigning IP addresses to instruments.

How BootP Service Works

Explains the BootP service process for instrument IP assignment.

Situation: Cannot Establish LAN Communication

Troubleshooting steps for failed LAN communication with BootP service.

Installation of BootP Service

Step-by-step guide for installing the Agilent BootP Service.

Two Methods to Determine the MAC Address

Methods to find MAC address via BootP logging or the LAN interface card label.

Assigning IP Addresses Using the Agilent BootP Service

Assigns IP addresses to instrument MAC addresses via the BootP service.

Changing the IP Address of an Instrument Using the Agilent BootP Service

Procedure to change IP address by stopping/restarting the BootP service.

Manual Configuration

Alters stored parameters in non-volatile memory via Telnet or Instant Pilot.

With Telnet

Configure TCP/IP parameters by opening a Telnet session to the module.

With the Instant Pilot (G4208 A)

Configure TCP/IP parameters using the Instant Pilot device.

PC and User Interface Software Setup Setup

Describes changing PC TCP/IP settings to match module defaults for local config.

User Interface Software Setup

Install user interface software according to the provided setup guide.

Appendix

General Safety Information

Explains safety symbols, warnings, and precautions for safe instrument operation.

Safety Standards

States instrument is Safety Class I, manufactured and tested to international standards.

Operation

General safety precautions during operation, service, and repair of the instrument.

The Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC)

Product compliance with WEEE Directive and information on proper disposal.

Radio Interference

Guidelines on using cables and ensuring radio interference limits are met.

Sound Emission

Manufacturer's declaration on sound pressure emission levels according to ISO 7779.

Agilent Technologies on Internet

Provides the worldwide web site for the latest product and service information.

Related product manuals