Table of contents
1 Information about the Manual .............................................................................................................. 6
1.1 Explanation of signs and symbols ..................................................................................................... 6
1.2 Disclaimer .......................................................................................................................................... 6
1.3 Copyright ............................................................................................................................................ 6
2 Safety ...................................................................................................................................................... 7
2.1 Explanation of the safety instructions ................................................................................................ 8
2.2 General safety instructions ................................................................................................................ 9
2.3 Repairs ............................................................................................................................................. 10
2.4 Intended use .................................................................................................................................... 10
2.5 Improper use .................................................................................................................................... 10
2.6 Safety symbols on the machine ....................................................................................................... 11
2.7 Emergency stop ............................................................................................................................... 12
2.8 Residual risks................................................................................................................................... 12
3 Description ........................................................................................................................................... 18
3.1 Front ................................................................................................................................................. 18
3.2 Back of the analyzer ........................................................................................................................ 19
4 Installation ............................................................................................................................................ 21
4.1 Setting up ......................................................................................................................................... 22
4.2 Filling the reagent tubes .................................................................................................................. 23
4.3 Establishing the gas supply ............................................................................................................. 23
4.4 Connecting the machine to the PC .................................................................................................. 24
4.5 Establishing the power supply ......................................................................................................... 24
5 Commissioning .................................................................................................................................... 25
6 Operation of the analyzer ................................................................................................................... 26
7 Technical data ...................................................................................................................................... 29
7.1 Technical data for the analyzer ........................................................................................................ 29
7.2 Type plate on the analyzer .............................................................................................................. 30
7.3 Standards for inorganic materials .................................................................................................... 31
8 Troubleshooting on the analyzer ....................................................................................................... 32
8.1 Troubleshooting on the analyzer. .................................................................................................... 32
9 Cleaning ............................................................................................................................................... 32
10 Maintenance ......................................................................................................................................... 33
10.1 Maintenance the analyzer ................................................................................................................ 33
10.1.1 Overview of maintenance work for the analyzer ...................................................................... 33
10.1.2 Removing the reagent tubes .................................................................................................... 34
10.1.3 Filling reagent tubes ................................................................................................................ 37
10.1.3.1 Filling the reagent tube on the SO
3
filter .......................................................................... 38
10.1.3.2 Filling the reagent tube on the inlet gas purification ........................................................ 39
10.1.3.3 Filling the reagent tube on the moisture filter .................................................................. 40
10.1.4 Inserting reagent tubes ............................................................................................................ 41
10.1.5 Replacing the dust filter cartridge on the analyzer .................................................................. 43
10.1.6 Filling the reagent tube on the catalyst furnace ....................................................................... 44
10.1.7 Cleaning the dust box .............................................................................................................. 47
10.1.7.1 Quick cleaning of the dust box ......................................................................................... 48
10.1.7.2 Thorough cleaning of the dust box .................................................................................. 49
10.1.8 Maintenance in the furnace area ............................................................................................. 50
10.1.8.1 Replacing the furnace cleaning brush and thermal shield ............................................... 50
10.1.8.2 Replacing the combustion tube ....................................................................................... 54
10.1.8.3 Removing the crucible tray .............................................................................................. 56
10.1.9 Replacing the O-rings .............................................................................................................. 57