6.31 NUTATE—Solids 2D Nutation
01-999162-00 C0402 VNMR 6.1C User Guide: Solid-State NMR
126
The 2D spectrum places chemical shift along F
2
and γB
1
along F
1
. Figure 60 is a diagram
of the sequence.
Macro
The macro nutate converts an S2PUL sequence parameter set into a 2D nutation
experiment.
Parameters
tpwr should be set so that a 90° pulse length should be about 50 kHz (or whatever other
value is desired).
sw1 controls the length of the tip angle, using as the increment value 1/sw1, in an
analogous way to all standard 2D experiments.
Processing
The data is processed by the command wft2d(0,0,0,1).
Reference
Samoson, A.; Lippmaa, E. J. Magn. Reson. 1988, 79, 255.
Figure 60. NUTATE Pulse Sequence
Tx
d1
d2
1.0s
0.0u
52.0m
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