01-999162-00 C0402 VNMR 6.1C User Guide: Solid-State NMR
128
Index
Index
Numerics
1 kW 1H/19F amplifier, 17
13C Chemical Shifts reference materials,
38
1H CRAMPS, 64, 65
1H/19F 1-kW amplifier,
57
3QMAS1 pulse sequence,
99
90× phase shift, 121
A
absolute position of CP/MAS rotor, 72
absolute-value plot, 90
Acquisition Controller board,
72
Acquisition Status window,
75
adamantane, 30
ADC (2 MHz or 5 MHz),
58
ADC conversion time,
47
adipic acid 1H CRAMPS spectrum, 65
adjusting
Hartmann-Hahn Match
CP/MAS probe,
36
homogeneity of sample,
29
magic angle,
32
air flow setting,
27
air supply,
72
amorphous silicon semiconductors,
93
amplifier blanking,
58
Amplifier Tuning,
57
ampmode, 18
AMT linear amplifier,
16, 47, 49
analyze command,
43, 83
analyze.inp text file, 83
angle measuring gauge,
32
angled brackets (< or >) notation,
12
Applications Laboratory, 13
AR linear amplifier,
47, 48
aromatic carbons magic angle adjustment,
32
attenuation, computer controlled, 50
automatic teller machine (ATM) cards caution,
10
B
bearing and drive pressures
Varian 5-mm CP/MAS probes,
24
Varian 7-mm CP/MAS probes,
24
bearing pressure and flowrate, 28
Bessel filter,
46, 47
biomolecular
materials structure definition,
106
structures determination,
111
blackened sector on rotor base,
74
blew parameter, 92
BLEW-12 cycles,
92
bmult parameter,
92
body nitrogen for solids probe VT operation, 78
booster power supply for VT controller,
78
BR24,
64, 69, 70, 71
Multacquisition Quardrature Correction, 67
pulse sequence,
69
C
C13EXCH pulse sequence, 90
calibrating
CP/MAS Probe,
35
13C Nucleus Pulse Width,
35
calibrate decoupler power,
36
Hartmann-Hahn match,
36
multipulse,
60–64
pulse width in wideline experiments, 52
carbon chemical shifts,
38
carbonyls magic angle adjustment,
32
cautions defined, 8
cavity tuned amplifier,
17
change bar,
12
change samples, 52
changing a rotor,
28
chemical shift
anisotropy (CSA),
14, 32
differences,
102
tensor components,
99
clock signal,
121
closed loop (C) mode,
77
closed-loop mode, rotor speed controller,
26
CMA amplifier,
17, 57
CMOS BIOS setup,
78
cntct parameter,
39, 86
cntct2 parameter,
115
coarse materials in a rotor,
22
Combined Rotation and Multipulse,
56
Complete Solids module, 15
composite echo,
118
compul parameter,
119
contact time, 81
array,
41
macro,
82
continuous mode amplifier operation, 48
conventions used in manual,
12
COSY pulse sequence,
103
CP/MAS
adjusting homogeneity,
29
adjusting the magic angle,
32
calibrating 13C pw90, 35
calibrating decoupler power,
36
experiments,
81
hardware,
16
hardware for 100/300 Watt Systems,
16
positioning the probe,
30
Solids Modules, 16
CP/MAS and CRAMPS,
59
CP/MAS probes and rotor speed control,
25
cp90 parameter, 90
cpcosyps macro,
103
CPCOSYPS pulse sequence,
103
cpcs macro, 102
CPCS pulse sequence,
102
CPI amplifier,
17, 57
CPNOESY experiment, 106
cpnoesyps macro,
105
CPNOESYPS pulse sequence,
104
CRAMPS, 56, 66
CRAMPS/multipulse,
57
CRAMPS/Multipulse Module,
56
CRAMPS/multipulse module hardware, 57
credit cards caution,
10
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