Varian Solid-State NMR - Page 131

Index
131 VNMR 6.1C User Guide: Solid-State NMR 01-999162-00 C0402
BR24, 67
multinuclear fast acquisition,
124
Multiple Pulse Line Narrowing (8-pulse cycle), 70
multiple-pulse
experiments,
81
selection, 102
multiple-quantum experiment,
123
Multipulse
capability,
57
Experiments,
56
Multipulse Tune-up Procedure,
60
90 degree pw calibration with FLIPFLIP, 61
prelimary calibrations,
61
removal of phase trasnsient with FLIPFLOP,
63
sample preparation, 60
spectrometer configuration,
61
N
nf parameter, 125
ni parameter,
124
nitrogen contact with body,
9
nitrogen gas flowmeters caution,
11
NOESY pulse sequence,
104
nonintegral spin quadrupolar nuclei,
14
non-narrowed spectra,
117
notational conventions,
12
noxious samples,
22
np parameter,
68
nuclear magnetic dipole,
14
nuclei,
117
nutate macro, 126
NUTATE pulse sequence,
125
nutation experiment,
125
O
observe
linear modulator setting,
40, 87
magnetization, 88
nucleus pulse calibration,
87
power setting,
39, 86
receiver board, 47
refocusing pulse,
109
selective-inversion pulse,
107
transmitter board, 50
OFF button,
50
off-resonance decoupling in solids,
42
Opella and Fry, 42
open loop (O) mode,
76
Operate button,
49
organic solids, 14
overdrive state,
58
P
p1 parameter, 69, 84, 107, 113, 119
p180 parameter,
40, 87, 119
p2 parameter,
81, 84, 89, 103
p3 parameter, 83, 84
pacemaker warning,
8
Pake doublet, 119
pass1 macro,
101
PASS1 pulse sequence, 101
PC-compatible computer,
76
pcrho parameter,
40, 87
pdp parameter, 40, 42, 82, 84, 87
pedestal and the image suppression,
66
periods parameter,
109
phase parameter, 89, 92, 104, 120
phase shift errors,
121
phase trasnsient removal with FLIPFLOP,
63
phase1 parameter, 68, 69
phase2 parameter,
68
phase-sensitive spectrum,
90
pMMA end caps, 20
pneumatics/tachometer box,
19, 76
description,
72
variable temperature version, 72
polarization transfer,
15
polycrystalline compounds,
14
polymers,
93, 119
Positioning the Probe,
30
powder
materials in a rotor,
21
pattern,
54
power button,
49
pp parameter,
109
preamplifier
solids,
59
programmed decoupling,
93
projectile hazard from spinning rotor,
22
prosthetic parts warning,
8
proton
-carbon heteronuclear chemical shift
correlation,
92
channel modulation, 95
chemical shift selection pulse,
92
multiple-quantum spectrum,
123
relaxation studies, 51
spin diffusion,
93
T
1
measurement, 44, 84
wideline experiments, 50
wideline spectrum,
93
protonated carbon suppression experiment,
42, 82
ptext command, 51
Pulse Sequence Controller board,
72, 121
Pulse Width and Phase Transient Calibration,
60, 68
pulse width calibration
CP/MAS,
35
CRAMPS,
61
wideline, 52
Pulsed button,
49
pulsed mode amplifier operation,
48
pw parameter, 68, 69, 70, 71, 84, 89, 92, 103, 104,
106, 118, 119, 120, 121, 122, 124
pw90
calibration using FLIPFLIP,
61
parameter,
52
pwx parameter,
88, 104, 106, 107, 111, 113, 115,
117