Varian Solid-State NMR - Page 7

List of Figures
7 VNMR 6.1C User Guide: Solid-State NMR 01-999162-00 C0402
Figure 41. 3QMAS1 Pulse Sequence .......................................................................................... 99
Figure 42. PASS1 Pulse Sequence ............................................................................................. 101
Figure 43. CPCS Pulse Sequence .............................................................................................. 102
Figure 44. CPCOSYPS Pulse Sequence .................................................................................... 104
Figure 45. CPNOESYPS Pulse Sequence ................................................................................. 105
Figure 46. R2SELPULS1 Pulse Sequence ................................................................................ 107
Figure 47. DIPSHFT1 Pulse Sequence ...................................................................................... 108
Figure 48. SEDRA2 Pulse Sequence ......................................................................................... 110
Figure 49. REDOR1 Pulse Sequence ........................................................................................ 112
Figure 50. DOUBLECP1 Pulse Sequence ................................................................................. 114
Figure 51. T1CP1 Pulse Sequence ............................................................................................. 115
Figure 52. HAHNCP1 Pulse Sequence ...................................................................................... 116
Figure 53. SSECHO1 Pulse Sequence ....................................................................................... 118
Figure 54. WLEXCH1 Pulse Sequence ..................................................................................... 120
Figure 55. HS90 Pulse Sequence ............................................................................................... 121
Figure 56. MREVCS Pulse Sequence ........................................................................................ 122
Figure 57. MQ_SOLIDS Pulse Sequence .................................................................................. 123
Figure 58. SPINDIFF Pulse Sequence ....................................................................................... 124
Figure 59. FASTACQ Pulse Sequence ....................................................................................... 125
Figure 60. NUTATE Pulse Sequence ......................................................................................... 126
List of Tables
Table 1. Background Nuclei of Rotor Material ............................................................................. 19
Table 2. Typical Spin Rates with Associated Bearing and Drive Values ....................................... 21
Table 3. Reference Materials and
13
C Chemical Shifts ................................................................. 32
Table 4. Bessel Filter Outputs ........................................................................................................ 35
Table 5. Wideline Experiment Commands and Parameters ........................................................... 38
Table 6. Rotor Synchronization Controls ...................................................................................... 53
Table 7. Rotor Controller Gain Setting and Typical Ranges ......................................................... 55
Table 8. Multiacquisition Quadrature Corrections for MREV8 .................................................... 99
Table 9. Multiacquisition Quadrature Corrections for BR24 ...................................................... 100
Table 10. Multiacquisition Quadrature Corrections for CORY24 ............................................... 100