Table of Contents 17
Chapter 5
Troubleshooting ............................................................................... 78
5.1 Troubleshooting Pump Problems .......................................... 78
5.2 Troubleshooting Noises......................................................... 84
5.3 Troubleshooting Chromatographic Problems ........................ 85
Appendix A
Specifications ................................................................................... 88
Appendix B
Spare Parts and Accessories ........................................................... 92
Appendix C
Solvent Considerations..................................................................... 96
C.1 Introduction .......................................................................... 96
C.2 Solvent Compatibility ........................................................... 97
C.3 Solvent Miscibility ................................................................ 99
C.4 Buffered Solvents .............................................................. 102
C.5 Head Height ...................................................................... 102
C.6 Solvent Viscosity ............................................................... 102
C.7 Mobile Phase Solvent Degassing ...................................... 102
C.7.1 Gas Solubility ......................................................... 103
C.7.2 Eluent Degassing Methods ..................................... 103
C.8 Wavelength Selection ........................................................ 105
Index ..................................................................................... 108