Table of Contents xiii
Shutting down the TQ Detector .................................................................. 2-15
Putting the TQ Detector in Standby mode for overnight shutdown........... 2-15
Complete TQ Detector shutdown.................................................................. 2-16
Emergency TQ Detector shutdown............................................................... 2-17
3 ESI and ESCi Modes of Operation ..................................................... 3-1
Introduction ....................................................................................................... 3-2
Installing the ESI probe .................................................................................. 3-2
Required materials .......................................................................................... 3-2
Installing the corona pin ................................................................................. 3-5
Required materials .......................................................................................... 3-5
Optimizing the ESI probe for ESCi operation ........................................... 3-7
Required materials .......................................................................................... 3-7
Removing the corona pin ................................................................................ 3-9
Required materials .......................................................................................... 3-9
Removing the ESI probe ............................................................................... 3-11
Required materials ........................................................................................ 3-11
4 Operating the Waters TQ Detector .................................................... 4-1
Setting-up the instrument .............................................................................. 4-2
Required materials .......................................................................................... 4-2
Performing a sample tune .............................................................................. 4-7
Required materials .......................................................................................... 4-7
Developing experiment methods .................................................................. 4-9
Required materials .......................................................................................... 4-9
Verifying the system using System QC ...................................................... 4-11
A Safety Advisories .................................................................................. A-1
Warning symbols ............................................................................................... A-2
Task-specific hazard warnings........................................................................ A-2
Warnings that apply to particular instruments, instrument components, and
sample types............................................................................................... A-3