Agilent Technologies 6490 - Page 107

Reference 6
Positive Ion Mode Checkout Conditions
Agilent 6400 Series Triple Quad LC/MS System Installation Guide 107
Tabl e 1 3 Source parameters
ESI (6410/6420/
6430/6460)
AJS (6460) AJS (6470) AJS (6490) AJS (6495)
Gas Temp 350°C 320°C 325°C 200°C 130°C
Gas Flow 13 L/min 10 L/min 10 L/min 12 L/min 11 L/min
Nebulizer 60 psi 20 psi 20 psi 20 psi 25 PSI
Sheath Gas Temp 400°C 400°C 400°C 400 C
Sheath Gas Flow 12 L/min 11 L/min 11 L/min 12 L/min
Nozzle Voltage 0 V 0 V 500 V 500 V
Tabl e 1 4 MS parameters
ESI (6410/6420/
6430/6460)
AJS (6460) AJS (6470) AJS (6490) AJS (6495)
Capillary 4000 V 4000 V 4000 V 3500 V 3500 V
Collision Energy 41 V41 V42 V41 V42 V
Fragmentor 150 V 195 V 195 V 380 V (fixed) 380 V (fixed)
Accelerator voltage 7 V 3 V 3 V 1 V 3 V
Delta EMV 200 V 200 V 200 V 200 V 200 V
Time Filtering 0.03 min 0.03 min 0.03 min 0.03 min 0.03 min
Compound Reserpine Reserpine Reserpine Reserpine Reserpine
Scan MRM MRM MRM MRM MRM
MS1 Res Unit Unit Unit Unit Unit
MS2 Res Unit Unit Unit Unit Unit
Precursor Ion 609.3 m/z 609.3 m/z 609.3 m/z 609.3 m/z 609.3 m/z
Product Ion 195.1 m/z 195.1 m/z 195.1 m/z 195.1 m/z 195.1 m/z
Dwell 200 ms 200 ms 200 ms 200 ms 200 ms
Low Pressure Funnel RF 110 V 110 V
High Pressure Funnel RF 200 V 200 V