Agilent Technologies 7683 - Filling Sample Vials; Vial Placement Without 100-vial Tray

Installation Guide
Making A Trial Run
13
Making A Trial Run
Once installation and configuration are complete, make a quick injection using
the sampler to verify that it works properly.
1. Install an empty syringe in the injector.
2. Place empty bottles in the Solvent A and Waste A turret positions. Place an
empty capped sample vial in the tray 1 position (or the turret sample 1
position, if not using the tray).
3. Set the following parameters on the GC:
4. Set the GC oven program to 25°C with a 0°C/min ramp, a hold time of
0.1 minutes, an equilibrium time of 0.3 minutes, and an initial time of
0.3 minutes.
Parameter Setting
Injection volume 1
# Sample pumps 1
Viscosity delay 0
# Sample washes 1
# Solv A washes 1
# Solv B washes 0
Slow plunger off
Pre-dwell time 0
Post-dwell time 0
Sampling offset off (on if cool on-column inlet used)
# Solv A pre-wash 1
# Solv B pre-wash 0
# Injections/vial 1
Samples 1–1*
*For 6890 GC with Agilent ChemStation control, enter 101–101.