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Agilent Technologies 7820A Advanced User's Guide

Agilent Technologies 7820A
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Detectors 5
Advanced User Guide 105
Helium, either as carrier or makeup gas, may cool the detector
gases below the ignition temperature. We recommend using
nitrogen rather than helium.
Lighting the FPD flame
Before trying to light the flame, have the detector at operating
temperature. Removing the condensate tubing may help, but be
sure to replace it before making runs.
It is difficult to light the flame with the flows shown in Table 20,
particularly in the sulfur mode. If the flame will not light with
the sulfur mode flows shown, change to the phosphorus mode
flows. After ignition, gradually reduce the flows to the sulfur
values. Some experimentation will be needed.
When either of the flame ignition methods in this section is
used, the FPD automatically performs this sequence:
1 Turns all detector gases—air, hydrogen, makeup—off. Carrier
remains on.
2 Sets air flow to 200 mL/min.
3 Turns the glow plug ignitor on.
4 Ramps the hydrogen flow from 10 to 70 mL/min.
5 Resets the air flow to the air flow setpoint.
6 Resets the hydrogen flow to the hydrogen flow setpoint.
7 Turns the makeup gas on.
8 Compares the signal change with the Lit offset value. If the
change is greater than Lit offset, declares the flame on (lit). If
it is less, declares the flame off (not lit).
For this process to work, there must be enough air pressure to
the pneumatics module to provide 200 mL/min flow. We
recommend a supply pressure of 90 psi.
Detector gases
Hydrogen 50 75
Air 60 100
Carrier + makeup 60 60
Table 21 Recommended flows (continued)
Sulfur mode flows,
mL/min
Phosphorus mode
flows, mL/min

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Agilent Technologies 7820A Specifications

General IconGeneral
BrandAgilent Technologies
Model7820A
CategoryLaboratory Equipment
LanguageEnglish

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