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Malvern Mastersizer 2000 User Manual

Malvern Mastersizer 2000
154 pages
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INSTRUMENTS
Printed in England MRK0864-01
Malvern Instruments Limited
Enigma Business Park
Grovewood Road, Malvern
Worcs, WR14 1XZ, U.K.
Tel: +44 (0) 1684 892456
Fax: +44 (0) 1684 892789
www.malvern.com
user manual
user manual
MastersizerMastersizer
Mastersizer
2000
2000

Table of Contents

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Malvern Mastersizer 2000 Specifications

General IconGeneral
Measurement PrincipleLaser diffraction
Data Acquisition RateUp to 10, 000 measurements per second
Power Requirements100-240 V AC, 50/60 Hz
Measurement Range0.02 - 2000 microns
Laser Wavelength633 nm (red)
Sample DispersionWet or dry
SoftwareMastersizer software
Optical ModelMie theory, Fraunhofer approximation
Weight25 kg
Detector arrangementMultiple detectors arranged to capture scattered light at various angles

Summary

Introduction to this manual

About this manual

Describes the manual's content, scope, and target audience.

Access to the instrument

Lists personnel roles and their responsibilities regarding instrument access.

Assumed information

Outlines general assumptions, naming conventions, and menu command structure.

Where to get help

Provides information on other manuals, help desk, and remote support options.

Overview

Introduction

Introduces the chapter's purpose: explaining the system's function and operation.

What the Mastersizer 2000 does

Explains the fundamental purpose of the Mastersizer in particle size analysis.

How the Mastersizer 2000 works

Details the underlying principles and procedures of the Mastersizer measurement process.

Making measurements

Describes the two methods for making measurements: SOPs and manual.

Viewing the results

Explains how measurement data is displayed in various report formats.

Saving the results

Details how to save measurement data into a measurement file.

Identifying the features

Introduction

Introduces the chapter covering the physical features of the Mastersizer system.

Typical systems

Illustrates common Mastersizer system configurations with key modules.

Optical bench components

Identifies and describes the main components of the optical bench.

Software

Outlines the main Mastersizer software interface and its features.

Making measurements - a tutorial

Introduction

Introduces the chapter on performing measurements, covering advice and procedures.

General measurement advice

Provides critical advice on sample preparation and cleanliness for accurate measurements.

The basics of making a measurement

Explains the two methods for making measurements: SOP and manual.

Measurements on a Mastersizer 2000

Details the steps for instrument preparation and making a basic SOP measurement.

Measurements on a Mastersizer 2000E

Details instrument preparation and SOP measurement for the Mastersizer 2000E.

Measuring new samples

Guides on setting up measurements for new materials using manual or SOP methods.

Measurement options

Explains the various dialogues and options available for measurement setup.

Viewing the results

Introduction

Introduces displaying and interpreting calculated measurement results.

Displaying the information

Explains how to open files and view records and reports in the measurement window.

Default reports

Lists and describes the standard reports provided by the Mastersizer software.

Changing the Records tab

Details how to customize the displayed fields in the Records tab.

Changing views - the Report Designer

Explains how to create custom reports using the Report Designer application.

Understanding the views

Introduction

Introduces the chapter on interpreting Mastersizer results and fundamental concepts.

Understanding the display

Explains how to interpret graphs like histograms and cumulative plots.

Report features

Describes key elements of a typical Mastersizer report, including statistics.

Fundamental concepts

Explains core concepts like concentration calculation and Beer-Lambert law.

Equivalent spheres

Discusses the concept of equivalent spheres in particle size measurement.

Derived distribution parameters

Details how distribution parameters and diameters are calculated.

Optical models

Contrasts Fraunhofer approximation with Mie theory used in Mastersizer.

Handling measurement files

Introduction

Outlines chapter topics: storage, sorting, exporting, and extracting SOPs.

Records and files

Explains the structure of records and measurement files, including re-analysis.

Searching and sorting records

Details how to search for records using criteria and sort them.

Exporting results

Covers various methods for exporting data to other applications.

Sample preparation

Introduction

Emphasizes the critical role of sample preparation for accurate results.

Sample preparation flow chart

Provides a visual guide for preparing unknown samples.

Representative sampling

Gives guidelines for ensuring the sample taken is representative of the whole.

Considerations for dry samples

Discusses specific factors and methods for preparing dry samples.

Considerations for wet samples

Covers choices and preparation methods for wet samples and dispersants.

Surfactants and admixtures

Explains the use of surfactants and admixtures to aid sample dispersion.

Bubbles

Discusses the issue of bubbles in the system and how to mitigate them.

Degassing

Explains the process and importance of degassing dispersants.

Symptoms of poor sample preparation

A table identifying common problems and their solutions.

Advanced features

Introduction

Introduces advanced features for experienced users to improve analyses.

Obscuration settings

Details how to set obscuration limits for detecting poor conditions.

Autodilution

Explains the automatic adjustment of sample concentration by adding dispersant.

Advanced result processing

Covers modifying results via transformation or reducing the result range.

Editing results

Explains how to re-analyze results with different parameters and save as a new record.

Defining user size bands

Describes how to customize particle size ranges for histograms and tables.

Alarms

Details setting cleanliness, alignment, and diameter alarms for monitoring.

Averaging records

Explains creating an average record from multiple measurements.

Importing results from older instruments

Covers viewing records from older Mastersizer versions.

Result emulation

Explains modifying results to emulate alternative sizing techniques.

Security

Introduction

Introduces the chapter on system security, principles, and user management.

Security principles

Outlines principles of user access, groups, and administrator roles.

Setting up the Administrator

Guides on configuring the administrator account and enabling security.

Security guidelines

Provides recommendations for secure user login and password management.

Setting up user groups

Details the process of creating and managing user groups and their permissions.

Setting up individual users

Explains how to define individual user properties, including username and group membership.

Appendix A Specification

Optical bench

Lists the detailed technical specifications for the Mastersizer optical bench.

Appendix B Chemical compatibility

Introduction

Discusses material compatibility with samples and dispersants within the system.

Appendix C Unpacking instructions

Appendix D Regulatory statements

CE Declaration of Conformity (APA2000)

Declares compliance with European Commission Directives for APA2000.

CE Declaration of Conformity (EPA2000)

Declares compliance with European Commission Directives for EPA2000.

FCC Notice (US only)

Provides FCC compliance information for Class A digital devices.

Canadian Regulatory Information (Canada Only)

Outlines digital apparatus compliance with Canadian Radio Interference Regulations.

VCCI acceptance (Japan only)

Indicates compliance with Japanese EMC regulations as specified by VCCI.

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