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PerkinElmer Spectrum 100 Series - User Manual

PerkinElmer Spectrum 100 Series
118 pages
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SPECTRUM 100 SERIES
User’s Guide
MOLECULAR SPECTROSCOPY

Table of Contents

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PerkinElmer Spectrum 100 Series Specifications

General IconGeneral
TypeFTIR Spectrometer
Spectral Range7800 to 350 cm-1
DetectorDTGS
BeamsplitterKBr
Light SourceHigh energy ceramic
Wavenumber Accuracy0.01 cm-1
Operating Temperature Range15°C to 35°C
Data CollectionSpectrum software
InterfaceUSB
Resolution0.5 cm-1

Summary

Introduction

About This Manual

Explains the manual's structure, content, and purpose.

Conventions Used in this Manual

Details text formatting, symbols, and terminology used throughout the guide.

Notes, Cautions and Warnings

Explains special notations for important information and safety alerts.

Warnings and Safety Information

Safety Summary

Provides a concise overview of critical safety precautions for instrument operation.

General Safety

Outlines general safety guidelines and environmental conditions for instrument use.

Electrical Safety

Covers essential electrical safety measures and connection guidelines.

Laser Safety Regulations

Explains regulations and safety precautions related to the instrument's laser system.

Use of Flammable Solvents and Samples

Provides critical safety instructions for handling flammable materials near the instrument.

An Overview of the Spectrometers

A Guided Tour of the Spectrum 100 Series

Provides a visual and descriptive walkthrough of the instrument's features.

Top Panel Controls

Explains the function of the display and go button on the instrument's top panel.

Sample Compartment

Describes the instrument's sample compartment and related precautions.

Optical System

Explains the instrument's optical system and its design for performance.

Unpacking and Installation

Requirements

Outlines necessary conditions and prerequisites before installing the instrument.

Environment

Details the ideal environmental conditions for optimal instrument performance.

Unpacking the Spectrometer

Provides step-by-step instructions for safely removing the instrument from its packaging.

Connecting to the PC

Guides the user on establishing a connection between the spectrometer and a PC.

Connecting the Spectrometer to the electrical supply

Instructs on how to safely connect the instrument to a power source.

Installing the Spectrum Software

Provides instructions for installing the necessary Spectrum software.

The Instrument Install Wizard

Guides the user through the automated process of installing the instrument.

Using the Spectrometer

Basics of Software Control

Introduces fundamental concepts for controlling the instrument via software.

Switching on the Spectrometer

Details the procedure for powering on the spectrometer and starting the software.

Controlling the Instrument

Explains how to operate the instrument and collect data using the software.

Atmospheric (CO2;H2 O) Suppression

Explains the feature for removing atmospheric interference from spectra.

Quality Checks

Introduces features for monitoring and ensuring spectral data quality.

Routine Maintenance

Cleaning the Spectrometer

Provides instructions for cleaning the exterior of the spectrometer.

The Desiccant Indicator

Explains the function and interpretation of the desiccant indicator.

Changing the Desiccant

Instructs on how to replace the desiccant packs to maintain instrument dryness.

Purging the Spectrometer

Explains how to purge the instrument with gas to remove moisture and CO2.

Cooling the MCT Detector (Spectrum 100)

Details the procedure for cooling the MCT detector with liquid nitrogen.

Advanced Maintenance

Opening the Main Cover

Guides on how to safely open the main cover for internal access.

Replacing the Source

Provides instructions for replacing the instrument's source.

Replacing the Beamsplitter

Details the procedure for replacing the beamsplitter component.

Replacing the Laser and Power Supply

Provides instructions for replacing the laser and its power supply unit.

Instrument Performance Validation

Principles of Use

Explains the underlying principles and regulatory requirements for instrument calibration.

Validating Instrument Calibration

Outlines the procedure for validating the instrument's calibration accuracy.

Printing the Certificate of Performance Validation

Details the process of generating and printing a performance validation certificate.

When Should I Recalibrate My Instrument?

Advises on when recalibration of the instrument is necessary.

Appendices

Appendix 1: Changing the Sampling Accessory

Provides detailed steps for swapping sampling accessories.

Appendix 2: Instrument Self-Checks

Explains the instrument's built-in self-check procedures.

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