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FatExtractor E-500
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88 pages
Manual
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BÜCHI Labortechnik AG
Installation | 5
Operation Manual FatExtractor E-500
41/88
Navigation path
➔
➔
[Settings]
➔
[Network]
u
Navigate to the action
[Network]
.
u
Enable the function
[DHCP]
.
ð
The instrument is prepared.
40
42
Table of Contents
Main Page
Default Chapter
3
Table of Contents
3
1 About this Document
7
Warning Notices in this Document
7
Symbols
7
Warning Symbols
7
Mark-Ups and Symbols
8
Trademarks
8
2 Safety
9
Proper Use
9
Use Other than Intended
9
Staff Qualification
9
Location of Warning Signs on the Product
10
Protection Devices
11
Residual Risks
11
Hot Surfaces
11
Empty Beakers on Heating Plates
11
Mechanical Damages
11
Glass Breakage
12
Glass Damages During Extraction Process
12
Overfilled Extraction Beakers
12
Spilled Hazardous Materials
12
Solvent Leakages During Extraction Process
12
Incorrect Function of the Analyte Protection Sensors
13
Traces of Dark Extracts or Residuals of Extract Foam
13
Personal Protective Equipment
13
Modifications
13
3 Product Description
14
Description of Function
14
Soxhlet Extraction
14
Hot Extraction
15
Economic Continuous Extraction
15
Description of the Analyte Protection Sensor (Option)
15
Configuration
16
Front View
16
Rear View
17
Upper Connections on the Rear Side
17
Lower Connections on the Rear Side
18
Installation Board
19
Interface
20
Pro Interface
21
Type Plate
21
Scope of Delivery
22
Technical Data
22
Fatextractor E-500
22
Ambient Conditions
23
Materials
24
4 Transport and Storage
25
Transport
25
Storage
25
Lifting the Instrument
25
5 Installation
27
Before Installation
27
Installation Site
27
Establishing Electrical Connections
27
Securing against Earthquakes
28
Connecting the Coolant Hose
28
Connecting the Solvent Tubes to the Condenser Tank Bottle
29
Connecting the Coolant Tubes to the Condenser Tank Bottle
30
Preparing the Tank Bottle
30
Preparing the Instrument for Soxhlet Extraction
31
Installations for Soxhlet Extraction
31
Preparing the Extraction Glass Chamber Soxhlet
31
Installing the Extraction Glass Chamber Soxhlet
32
Preparing the Instrument for Hot Extraction
33
Installations for Hot Extraction
33
Preparing the Instrument for Economic Continuous Extraction
34
Installations for Economic Continuous Extraction
34
Preparing the Extraction Glass Chamber for an Economic Continuous Extraction
34
Installing the Extraction Glass Chamber Economic Continuous Extraction
34
Installing the Protection Shields
35
Installing Two Protection Shields (Soxhlet Only)
35
Installing One Protection Shield (Hot and Economic Continuous Extraction Only)
36
Preparing the Condenser
36
Selecting a Configuration
39
Disassembling the Condenser Circuit
39
Mobile Connection
40
Requirements for Local Network Settings
40
Preparing the Instrument for App Using
40
6 Operating the Interface
42
Layout of the Interface
42
Function Bar
42
Menu Bar
43
Home Menu
44
Method Menu
44
Configuration Menu
44
Solvent Menu
47
Status Bar
47
7 Operating the Interface Pro
48
Layout of the Interface
48
Function Bar
48
Menu Bar
49
Home Menu
50
Method Menu
50
Configuration Menu
51
Solvent Menu
53
Status Bar
53
8 Editing a Method
54
Creating a New Method
54
Changing the Name of a Method
54
Setting the Solvent of a Method
54
Setting the Extraction Time of a Method
55
Setting the Extraction Cycles of a Method (Soxhlet Extraction Only)
55
Setting the Extraction Heating Level of a Method
56
Setting the Soxhlet Valve Open Time of a Method (Soxhlet Only)
56
Setting the Rinse Time of a Method (Soxhlet and Hot Extraction Only)
57
Setting the Rinse Heating Level of a Method (Soxhlet and Hot Extraction Only)
57
Setting the Number of Drains for a Method (Hot Extraction Only)
58
Setting Smartdrying (Soxhlet and Economic Continuous Extraction Only)
58
Setting the Drying Time of a Method
59
Setting the Drying Heating Level of a Method
59
9 Performing an Extraction
61
Task During Performing an Extraction
61
Adding Solvent through the Condenser
61
Putting the Glass Sample Tube with Frit in the Extraction Glass Chamber
62
Performing a Soxhlet Extraction
63
Adjusting the Optical Sensor on the Extraction Glass Chamber Soxhlet
63
Preparing the Instrument for a Soxhlet Extraction
63
Selecting a Method
63
Selecting the Extraction Positions
64
Starting a Soxhlet Extraction
64
Ending a Soxhlet Extraction
65
Shutting down the Instrument
65
Performing a Hot Extraction
66
Preparing the Instrument for a Hot Extraction
66
Selecting a Method
66
Selecting the Extraction Positions
66
Starting a Hot Extraction
67
Ending a Hot Extraction
67
Shutting down the Instrument
68
Performing an Economic Continuous Extraction
68
Preparing the Instrument for an Economic Continuous Extraction
68
Selecting a Method
68
Selecting the Extraction Positions
68
Starting an Economic Continuous Extraction
69
Ending an Economic Continuous Extraction
70
Shutting down the Instrument
70
Exporting Extraction Parameters
70
Exporting Extraction Parameters Without Cloud Connection
70
Exporting Extraction Parameters with Cloud Connection
71
10 Editing a Solvent
72
Creating a New Solvent
72
Changing the Name of a Solvent (Own Created Solvents Only)
72
11 Cleaning and Servicing
73
Regular Maintenance Work
73
Removing the Tank Bottle
74
Draining Solvent from the Instrument
75
Switch on the Pump
75
Open the Tank Valves
75
Switch of the Pump
76
Draining Solvent from Extraction Glass Chamber (Soxhlet Only)
76
12 Help with Faults
77
Troubleshooting
77
Draining Solvent from Extraction Glass Chamber (Soxhlet Only)
79
13 Taking out of Service and Disposal
80
Taking out of Service
80
Disposal
80
Returning the Instrument
80
14 Appendix
81
Schematics
81
Condenser Circuit
81
Solvent Collector Schematic
82
Spare Parts and Accessories
82
Spare Parts
82
Conversion and Upgrade Kits
84
Accessories
85
Holder for Extraction Thimbles
85
Glass Sample Tubes and Extraction Thimbles
86
Documentation
87
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