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TA Instruments DSC Autosampler CE User Manual

TA Instruments DSC Autosampler CE
190 pages
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TA I
NSTRUMENTS
DSC A
UTOSAMPLER
CE i
DSC
Autosampler
CE
Operator’s Manual
PN 825616.001 Rev. B (Text and Binder)
PN 825616.002 Rev. B (Text Only)
Issued November 1999
109 Lukens Drive New Castle, DE 19720
Thermal Analysis & Rheology
A S
UBSIDIARY
OF
W
ATERS
C
ORPORATION

Table of Contents

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TA Instruments DSC Autosampler CE Specifications

General IconGeneral
CategoryLaboratory Equipment
ManufacturerTA Instruments
ModelDSC Autosampler CE
ApplicationAutomated sample handling for DSC analysis
Sample CapacityUp to 54 samples
Power Requirements100-240 VAC, 50/60 Hz
TypeDifferential Scanning Calorimeter (DSC) Autosampler
CompatibilityTA Instruments DSC series instruments
AutomationFully automated sample loading and unloading
Temperature RangeTypically matches the DSC instrument range (-180°C to 725°C, depending on DSC model)
Cooling MethodDependent on the DSC instrument connected
Heating RateDependent on the DSC instrument connected
Cooling RateDependent on the DSC instrument connected
Temperature AccuracyDependent on the DSC instrument connected
Temperature PrecisionDependent on the DSC instrument connected
Calorimetric SensitivityDependent on the DSC instrument connected
Data Sampling RateDependent on the DSC instrument connected
Atmosphere ControlNitrogen, Argon
Software CompatibilityTA Instruments software

Summary

Safety, Introduction, and Preparation

Safety and Handling Precautions

Notes, cautions, warnings, CE compliance, and safe lifting procedures.

Introduction to DSC Autosampler CE

Overview, features, components, system relationship, requirements, and terminology.

Initial Setup and Preparation

Steps for unpacking, connecting, installing lids, and dust cover.

Operation, Calibration, and Diagnostics

Manual Mode Operation

Using the autosampler in manual mode: starting, mode switching, turret control, pan handling.

Calibration Procedures and Tests

Step-by-step guide for calibrating positions and performing diagnostic tests.

Diagnostics and Error Handling

Performing diagnostic tests and resolving error messages.

Sample Preparation and Reference

Sample Preparation

Installing crimping die, setting up tray, preparing sample pans (crimped/hermetic).

Reference Information

Lists of parts, supplies, ordering information, and document index.

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