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Agilent Technologies 7000 Triple Quadrupole GC/MS User Manual

Agilent Technologies 7000 Triple Quadrupole GC/MS
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General Troubleshooting 2
Troubleshooting and Maintenance Manual 47
Air Leaks
Air leaks are a problem for any instrument that requires a vacuum to operate.
Leaks are generally caused by vacuum seals that are damaged or not fastened
correctly. Symptoms of leaks include:
Higher than normal analyzer chamber pressure or foreline pressure
Higher than normal background
Peaks characteristic of air (m/z 18, 28, 32, and 44 or m/z 14 and 16)
Poor sensitivity
Low relative abundance of m/z 502 (this varies with the tune program used)
Leaks can occur in either the GC or the MS. The most likely point for an air
leak is a seal you recently opened.
In the GC, most leaks occur in:
GC inlet septum
GC inlet column nut
Broken or cracked capillary column
Leaks can occur in many more places in the MS:
GC/MS interface column nut
Side plate O-rings (all the way around)
Vent valve O-ring
Calibration valve
GC/MS interface O-ring (where the interface attaches to the analyzer
chamber)
Front and rear end plate O-rings
Turbo pump O-rings
Collision cell cover O-ring

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Agilent Technologies 7000 Triple Quadrupole GC/MS Specifications

General IconGeneral
BrandAgilent Technologies
Model7000 Triple Quadrupole GC/MS
CategoryLaboratory Equipment
LanguageEnglish

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