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G7117C
Agilent Technologies G7117C User Manual
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Agilent InfinityLab LC Series Diode Array D
e
tectors User Manual
103
5
Optimizing the Detector
Warm up of the Detector
Figure
31
Detector W
arm-up – 1
st
hour
Figure
32
Detector W
arm-up – 2
nd
hour
102
104
Table of Contents
Table of Contents
5
1 Introduction
9
Overview of the Module
10
Product Description
11
Product Description G7117A
11
Product Description G7117B
12
Product Description G7117C
13
Optical System
14
Lamp
15
Max-Light Cartridge Flow Cell
15
Slit Assembly
16
Grating and Diode Array
18
Leak and Waste Handling
19
Waste Concept
23
Operating Principle
24
2 Site Requirements and Specifications
25
Site Requirements
26
Physical Specifications
29
Performance Specifications
30
Specifications
30
Specification Conditions
36
3 Using the Module
37
Magnets
38
Turn On/Off
39
Status Indicators
41
Instrument Configuration
42
Set up the Detector with Agilent Open Lab Chemstation
44
The Detector User Interface
45
Detector Control Settings
47
Method Parameter Settings
48
4 Preparing the Module
52
Leak and Waste Handling
53
Waste Concept
54
Before Using the System
55
Setting up an Analysis
55
Requirements and Conditions
57
Preparing the Detector
59
Preparing the HPLC System
59
Running the Sample and Verifying the Results
61
Solvent Information
62
Capillary Coding Guide
68
Syntax for Capillary Description
68
At-A-Glance Color-Coding Keys
70
Installing Capillaries
71
5 Optimizing the Detector
75
Introduction
76
Optimization Overview
77
Choosing a Flow Cell
78
Inline Pressure Relief Valve Kit (G4212-68001)
81
Application Information
81
Special Information of 60 MM Cartridge Flow Cell
81
Optimizing for Sensitivity, Selectivity, Linearity and Dispersion
83
Flow Cell Path Length
83
Peak Width (Response Time)
85
Sample and Reference Wavelength and Bandwidth
87
Slit Width (G7117B)
90
Optimizing Spectral Acquisition
92
Margin for Negative Absorbance
93
Optimizing Selectivity
94
Quantifying Coeluting Peaks by Peak Suppression
94
Optimizing the Detector Regarding to the System
96
Delay Volume and Extra-Column Volume
96
How to Configure the Optimum Delay Volume
96
How to Achieve Higher Sensitivity
97
Warm up of the Detector
102
6 Troubleshooting and Diagnostics
104
Available Tests Vs User Interfaces
105
Agilent Lab Advisor Software
107
7 Error Information
108
What Are Error Messages
109
General Error Messages
110
Timeout
110
Shutdown
110
Remote Timeout
111
Lost CAN Partner
111
Leak Sensor Short
112
Leak Sensor Open
112
Compensation Sensor Open
113
Compensation Sensor Short
113
Fan Failed
114
Leak
114
Open Cover
115
Cover Violation
115
ERI Messages
115
Detector Error Messages
116
Diode Current Leakage
116
UV Lamp Current
116
UV Lamp Voltage
117
UV Ignition Failed
117
UV Heater Current
118
Calibration Values Invalid
118
Wavelength Recalibration Lost
119
Illegal Temperature Value from Sensor on Main Board
119
Illegal Temperature Value from Sensor at Air Inlet
120
Heater at Fan Assembly Failed
120
Heater Power at Limit
120
8 Test Functions and Calibration
121
Introduction
122
Use of Max-Light Cartridge Test Cell
126
Conditions of Detector
127
Failing a Test
127
Self-Test
128
Intensity Test
130
Test Failed
131
Cell Test
132
Test Failed (Low Ratio Value)
133
Quick Noise Test
134
Test Failed
136
ASTM Drift and Noise Test
137
Test Failed
139
Slit Test
140
Slit Test (G7117B)
140
Test Failed
141
Slit Test (G7117A/G7117C)
142
Wavelength Verification Test
143
Wavelength Calibration
145
Wavelength Recalibration Fails
147
D/A Converter (DAC) Test
148
Test Evaluation
149
Dark Current Test
150
Test Failed
151
Emfs - Early Maintenance Feature
152
Other Lab Advisor Functions
152
9 Maintenance
153
Default Chapter
154
Introduction to Maintenance
154
Warnings and Cautions
154
Overview of Maintenance
156
Cleaning the Module
157
Remove and Install Doors
157
Replace the Deuterium Lamp
159
Replace the Max-Light Cartridge Cell
162
Clean the Max-Light Cartridge Cell
165
Storage of Max-Light Cartridge Cell
166
Correcting Leaks
167
Replace Leak Handling System Parts
168
Replace the Module Firmware
170
Information from Module's Assemblies
171
10 Parts and Materials for Maintenance
172
Overview of Maintenance Parts Accessory Kit
172
11 Identifying Cables
175
Cable Overview
176
Analog Cables
178
Remote Cables
180
CAN/LAN Cables
183
Cables
184
USB Cables
184
12 Hardware Information
185
Firmware Description
186
Electrical Connections
189
Information on Instrument Serial Number
190
Interfaces
192
Rear View of the Module
190
Overview Interfaces
194
ERI (Enhanced Remote Interface)
196
USB (Universal Serial Bus)
198
Setting the 6-Bit Configuration Switch
199
Special Settings
200
Instrument Layout
202
Early Maintenance Feedback
203
13 LAN Configuration
205
What You Have to Do First
206
TCP/IP Parameter Configuration
207
Configuration Switches
208
Initialization Mode Selection
209
Dynamic Host Configuration Protocol (DHCP)
211
General Information (DHCP) Setup (DHCP)
211
Manual Configuration
214
With Telnet
215
With the Instant Pilot (G4208A)
218
14 Appendix
219
General
220
General Safety Information
220
Safety Standards
220
Before Applying Power
221
Ground the Instrument
221
Do Not Modify the Instrument
222
Do Not Operate in an Explosive Atmosphere
222
Do Not Remove the Instrument Cover
222
In Case of Damage
222
Solvents
223
Safety Symbols
224
Waste Electrical and Electronic Equipment (WEEE) Directive
226
Radio Interference
227
Sound Emission
227
Solvent Information
228
Agilent Technologies on Internet
229
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Agilent Technologies G7117C Specifications
General
Brand
Agilent Technologies
Model
G7117C
Category
Laboratory Equipment
Language
English
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