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709-DS
Agilent Technologies 709-DS User Manual
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15
Agilent T
echnologies
708-DS / 709-DS Dissolution Apparatus
Operator’s Manual
2
Intr
oduction
Conventions Used in this Manual
17
Serial Number Format
18
14
16
Table of Contents
Default Chapter
3
Default Chapter
3
Table of Contents
3
Figures
7
Tables
9
1 Safety
11
Electrical Hazards
11
Warning
13
Caution
13
Note
13
Information Symbols
14
2 Introduction
15
Conventions Used in this Manual
17
Serial Number Format
18
3 Setting up the 708-DS / 709-DS
19
Initial Setup
20
Unpacking Procedure
20
Figure 1 Unpacking
20
Figure 2 Removing the Apparatus
21
Environmental Requirements for Installation
22
Clearance
22
Equipment, Parts, and Accessories as Shipped
23
Parts and Accessories
23
Tubing / Cable Connections
24
Heater / Circulator Setup (708-DS)
24
Figure 3 BATH HEATER Connector
24
Instrument Level / Water Bath Setup
25
Level Instrument
25
Figure 4 Levelers and Stability Feet
25
Figure 5 Level-Adjustment Screw Caps
26
Figure 6 Raising the Stability Feet
27
DVH Power Controller Setup (709-DS)
28
Figure 7 DVH Power Controller
28
Temperature Probe Installation (708-DS)
29
Figure 8 BATH TEMP Connector
29
Figure 9 Positioning the Temperature Probe
29
EVT Probe Installation (708-DS)
30
Power Cord Connections
30
708-DS / 709-DS Initial Power up
30
Filling the Water Bath (708-DS)
31
Figure 10 Filling the Water Bath
31
Level Instrument - Re-Verification
32
Heater / Circulator Power-Up (708-DS)
32
Agilent 708-DS / 709-DS Setup
33
Vessel Isolation Chamber Installation (709-DS)
33
Vessel Installation
34
Figure 11 Vessel Bubble
34
Sample Manifold Installation
35
Figure 12 Positioning the Manifold for Installation
35
Figure 13 Connecting Autotemp
36
Accessory Installation
37
Figure 14 Affixing the Fasteners
37
Figure 15 Proper Sample Tubing Position
38
Figure 16 Installing Evaporation Covers on Shafts
39
Figure 17 Shaft Locking Collars
39
Figure 18 Dosage Delivery Module and Alignment Post
40
Figure 19 Inserting DDM into DDM Alignment Shaft
41
Figure 20 Attaching DDM to Alignment Post
42
Setting Basket (Apparatus 1) Heights
43
Figure 21 Accessory Installation
43
Setting Paddle (Apparatus 2) Heights
44
Figure 22 Tightening the Shaft Locking Collar
44
Figure 23 Inserting Height Spheres
45
4 Operating the 708-DS / 709-DS
47
Main Screen - Options
48
Main Screen - Display Parameters
48
Figure 24 Main Screen - Display Parameters
48
Main Screen - Sample Temperatures
49
Main Screen - Run
50
Table 1 Method - Start Options
52
Main Screen - Stop
57
Main Screen - Drive Unit up / down
59
Manual Drive Unit up / down
60
Figure 25 Manual Lift Knob
60
Manual Sampling
61
Figure 26 Taking a Manual Sample
61
Main Screen - Manifold up / down
62
Figure 27. Agilent 708-DS / 709-DS Standard Evaporation
62
Main Screen - Lock
63
Main Screen - Unlock
64
Main Screen - Remote Control
65
Main Screen - Alarms
65
Main Screen - Maintenance Due Icon
66
Menu Screen - System Menu
67
Menu Screen - Method Editor
68
Table 2 Method Properties Screen
69
Table 3 Method Properties Screen
70
Menu Screen - Reports
77
Menu Screen - Alarms
80
Table 5 Menu Screen - Alarms
80
Menu Screen - Instrument
82
Table 6 Menu Screen - Instrument Settings Screen
82
Menu Screen - Calibration
87
Menu Screen - Diagnostics
90
Table 10 Menu Screen - Diagnostics Screen 1
90
Table 12 Diagnostics - DVH Diagnostics Screen 1
93
Menu Screen - User Access
95
General 708-DS / 709-DS Conventions
96
Alphanumeric Data Entry
96
Numeric and Time / Date Entry
97
Table 13 Numeric and Time / Date Entry
97
Parameter Limits / Ranges
98
Table 14 Parameter Limits / Ranges
98
Table 4. Method Properties Screen
99
Agilent 708-DS / 709-DS Notifications
100
Main Screen - Error Conditions
100
Dialog Screens (Green / Blue)
102
Table 15 Dialog Screens (Green / Blue)
102
Warning Screens (Yellow)
104
Table 16 Warning Screens (Yellow)
104
Error Screens (Red)
109
Table 17 Error Screens (Red)
109
5 Maintenance and Troubleshooting
115
Preventive Maintenance
116
Weekly Maintenance
116
Monthly Maintenance
116
Bi-Annual Maintenance
116
Sample Line / Paddle / Basket Care
117
Shafts
117
Baskets
118
Rinsing Sample Lines
119
Rinse Cups (Optional)
120
Figure 28 Rinse Cup
120
Vessels and Evaporation Covers
122
DVH Vessel Care (709-DS)
122
Water Bath Care
122
Water Bath and Temperature Probes (708-DS)
123
Water Bath Temperature Probe Accuracy Test
123
Figure 29 Resistance Value of Temperature Probe
125
Removing or Adjusting Cannulas / Probes
126
Manifold Maintenance
126
Removing the Manifold
126
Accessing the Top Cover
127
Removing Top Cover
127
Replacing the Top Cover
127
Printer Maintenance
128
Removing a Thermal Paper Roll
128
Figure 30 Near-Empty Paper Roll
128
Figure 31 Accessing the Printer Handle
129
Figure 32 Open Printer Chamber
129
Inserting a Thermal Paper Roll (5095-0307)
130
Figure 33 Removing the Thermal Paper Roll
130
Figure 34 Inserting a Thermal New Paper Roll
131
Figure 35 Leading Paper and Closing the Lid
132
Figure 36 Closing the Printer Chamber
132
Figure 37 Feeding Paper
133
Thermal Printer Test
134
Figure 38 Printer Test
134
Obtaining Warranty and Other Services
135
Index
137
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Agilent Technologies 709-DS Specifications
General
Brand
Agilent Technologies
Model
709-DS
Category
Laboratory Equipment
Language
English
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