Shimadzu PDA-7000 - 4.6 Content analysis

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Chapter 3

Starting and Stopping the Instrument

Main Page

Introduction3
Indications Used in this Manual5
Warning Labels6
Safety Instructions7
Installation Site7
Installation7
Operation8
In an Emergency10
During a Power Outage10
Handling High-Pressure Gas11
Warranty13
After-Sales Service and Availability of Replacement Parts14
Disposal Precautions15
Table of Contents16
Definition of Terminology20
Parts List21
Checking of Parts21
Consumables and Maintenance Parts22
Repair Parts23
How to Distinguish Similar Parts24
Configuration and Function of the Instrument25
Switch Panel27
Spark Stand29
Spectrometer31
Condenser Lens31
Temperature Control Circuit31
Lamp32
Evacuation System32
Read-Out Unit33
Photo Detector (PMT)33
Photo Detector Sensitivity Controller (Attenuator)33
Integrator33
Data Processor System34
Specification38
Spectrometer38
Excitation Unit38
Spark Stand38
Excitatiion Source Unit38
Read-Out Unit39
Data Processor System39
Hardware39
Software40
Starting and Stopping the Instrument43
Inspection before Using the Instrument44
Starting the Instrument (Daily Use)45
Starting the Instrument after It Has Not Been Used for a Long Time46
Shutting down the Instrument (Daily Use)47
Shutting down the Instrument for a Long Time48
Emergency Stop and Recovering49
Emergency Stop49
Recovering from Emergency Stop50
Operation51
Argon Gas Bubbler52
Checking Gas Flow Rate54
When the Instrument Is in Operation54
When the Instrument Is Not Used or at Nighttime55
Turning on / off Photo Detector56
Sample Pretreatment57
Setting the Sample59
Content Analysis60
Recalibration61
Master Curve Recalibration63
Check Analysis64
Maintenance65
Maintenance and Inspection Items66
Periodical Maintenance66
Other Maintenance66
Work Required after Maintenance Service67
Maintenance Service by Shimadzu Service Engineer67
Maintenance Flow68
Maintaining the Spark Stand69
Maintenance Cycle70
Maintenance Procedure72
Exchanging the Electrode O-Ring82
Cleaning the Condenser Lens83
Adjusting the Control Gap87
Replacing Pump Oil90
Manual Scanning91
Lamp Test93
Waste Discharge94
File Utility95
Saving (Backup)95
Loading (Restoration)96
Replacing Recalibration Samples97
Replacing Argon Gas Cylinder98
Periodic Inspection98
Cleaning the Temperature Control Fan Heater98
Installation102
Temperature and Humidity102
Vibration102
Dust102
Grounding102
Power Supply103
Argon Gas103
Exhaust Equipment103
Peripheral Equipment104
Other Environmental Requirement104
Moving and Disposing of the Product104
Troubleshooting105
Basic Items to be Checked106
Troubleshooting106
Installing the Software108

Shimadzu PDA-7000 - 4.6 Content analysis

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