Siemens PGC 302 Edition II - DETECTORS edition II; Igniting FID;FPD, switching-on TCD; Adjusting the TCD bridge; New integration procedures and other improvements

CONTENTS
Page
DETECTORS edition II
Igniting FID/FPD, switching-on TCD . . . . . . . . 4
Switching off the TCD bridge current . . . . . . . . 5
Adjusting the detector current . . . . . . . . . . . . . 5
TCD status display . . . . . . . . . . . . . . . . . . 5
Changing the polarity of the TCD signal . . . . . . . 5
Compensating the baseline current
Adjusting the TCD bridge . . . . . . . . . . . . . . . 5
Selecting the range . . . . . . . . . . . . . . . . . . 6
Baseline monitoring . . . . . . . . . . . . . . . . . . 6
CHROMATOGRAPHS edition II :
CHROMATOGRAM ON THE
RECORDER
Extending the analog outputs . . . . . . . . . . . . . 8
Converting the analog outputs . . . . . . . . . . . . 8
Attenuation . . . . . . . . . . . . . . . . . . . . . . 9
Changing the polarity . . . . . . . . . . . . . . . . 10
Damping . . . . . . . . . . . . . . . . . . . . . . . 10
Baseline offset . . . . . . . . . . . . . . . . . . . . 10
Baseline correction . . . . . . . . . . . . . . . . . 11
Triggering a baseline correction . . . . . . . . . . . 11
Cancelling the baseline correction . . . . . . . . . 11
New integration procedures
and other improvements
Selecting the integration procedure . . . . . . . . 12
100 % over all peaks: area standardization . . . . . 13
External standard . . . . . . . . . . . . . . . . . . 13
100 % over all components . . . . . . . . . . . . . 13
Mixed mode . . . . . . . . . . . . . . . . . . . . . 14
Internal standard (only laboratory version) . . . . . 14
External standard (only laboratory version) . . . . 15
Three new time events program parameters . . 16
Switching over the peak width . . . . . . . . . . . 16
Drawing baseline from trough to trough . . . . . . 16
Terminate integration prematurely . . . . . . . . . 16
Page
Reintegration new!
Switching the automatic raw data
transmission on or off . . . . . . . . . . . . . . . . 18
Run longer than 20 minutes?
Define compression factor . . . . . . . . . . . . . 18
Increasing the compression . . . . . . . . . . . . . 18
Shifting the start of raw data storage . . . . . . . . 18
Selecting the run . . . . . . . . . . . . . . . . . . 19
Viewing the chromatogram or result . . . . . . . . 19
Optimizing the integration parameters . . . . . . . 20
Reintegration at desk without chromatograph . . . 20
Further useful information . . . . . . . . . . . . . 21
Print the chromatogram
and results following each run
Installation . . . . . . . . . . . . . . . . . . . . . . 22
Hardware requirements . . . . . . . . . . . . . . . 22
Switching the automatic printing on or off . . . . . 22
Optimization of time events program
for chromatogram printout . . . . . . . . . . . 23
Switchover time . . . . . . . . . . . . . . . . . . . 23
Measuring range . . . . . . . . . . . . . . . . . . . 23
Chart drive . . . . . . . . . . . . . . . . . . . . . . 23
Baseline offset . . . . . . . . . . . . . . . . . . . . 23
Test printout . . . . . . . . . . . . . . . . . . . . . 24
Manual printout of chromatogram . . . . . . . . . 24
Faults when printing . . . . . . . . . . . . . . . . 24
Manual printing of results . . . . . . . . . . . . . 25
Miscellaneous
Date/time . . . . . . . . . . . . . . . . . . . . . . 26
Baseline monitoring . . . . . . . . . . . . . . . . . 26
Temperatures and cooling . . . . . . . . . . . . . . 26
Analytical method . . . . . . . . . . . . . . . . . . 26
Analog inputs and outputs . . . . . . . . . . . . . 26
Display Peak recognition modified . . . . . . . . . 27
Display Raw data/Print modified . . . . . . . . . . 27
Correction of errors in Register 5, V5.0 . . . . . . 28
Contents
5INHALT.CHP, Stand Dezember 22, 1999
3