24 Agilent 1100 Series Fraction Collectors User’s Guide
1 Configuration and Operation of the Fraction Collector
Delay volumes and delay calibration
21 Perform the calibration again. Verify the time is sufficient (>5 seconds, see
Figure 8).
22 Press the Calibrate button if you want to store the new calculated delay
volume for the MSD in the Fraction Collector Configuration (see also
“Configuration of the Fraction Collector in the ChemStation” on page 10).
23 Press the Print button to get a hard copy of the report.
24 Stop the splitter.
25 Return to the Method and Run Control View and load the method you will
be using to run your samples. Select Fraction Collection from the More
MSD... sub-menu under the Instrument menu
Press the Parameters button and enter the final calculated delay time that
appears in the report in the Collector Delay field, first converting it to
minutes. In this case you would enter 11.991/60 = 0.20 minutes (see Figure 9).
Figure 8 Delay time greater than 5 seconds
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