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883 Basic IC plus
Metrohm 883 Basic IC plus User Manual
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883 Basic IC plus
2.883.0020
Manual
8.883.8001EN / 2019-
12-
12
2
Table of Contents
Default Chapter
5
Table of Contents
5
1 Introduction
9
Instrument Description
9
Intended Use
10
Safety Instructions
11
General Notes on Safety
11
Electrical Safety
11
Tubing and Capillary Connections
12
Flammable Solvents and Chemicals
12
Recycling and Disposal
12
Symbols and Conventions
13
2 Overview of the Instrument
14
Front
14
Figure 1 883 Basic IC Plus Front
14
Rear
15
Figure 2 883 Basic IC Plus Rear
15
3 Installation
16
About this Chapter
16
Initial Installation
16
Installation Diagram
19
Figure 3 Installation Diagram 883 Basic IC Plus
20
Setting up the Instrument
22
Packaging
22
Checks
22
Location
22
Capillary Connections in the IC System
22
Installations on the Rear of the Instrument
25
Positioning and Connecting the Detector
25
Figure 4 Positioning the Detector
25
Transport Locking Screws
26
Installing the Drainage Tubing
27
Figure 5 Drainage Tubing
28
Capillary and Cable Feed-Throughs
29
Figure 6 Capillary Feed-Throughs on the Door
30
Connecting the Eluent Bottle
31
Figure 7 Installing the Eluent Bottle Cap
31
Figure 8 Installing Tubing Weighting and Aspiration Filter
33
Installing the High-Pressure Pump
35
Installing an Inline Filter
35
Figure 9 High-Pressure Pump with Purge Valve
35
Installing the Pulsation Absorber
36
Figure 10 Inline Filter
36
Figure 11 Pulsation Absorber
36
Injection Valve
37
Figure 12 Exchanging the Sample Loop
38
Suppressor
39
General Information on the Suppressor
39
Installing the Suppressor
39
Connecting the Suppressor
41
Figure 13 Suppressor - Connection Capillaries
42
Peristaltic Pump
46
Installing the Peristaltic Pump
46
Figure 14 Peristaltic Pump
46
Mode of Operation for the Peristaltic Pump
50
Conductivity Detector
51
Figure 15 Front of Conductivity Detector
51
Figure 16 Rear of Conductivity Detector
52
Connecting the Instrument to a Computer
53
Figure 17 Connection Detector-MSM
53
Connecting the Instrument to the Power Grid
54
Initial Start-Up
55
Connecting and Rinsing the Guard Column
57
Connecting the Separation Column
59
Conditioning
62
4 Operation and Maintenance
64
IC System
64
Operation
64
Care
64
Maintenance by Metrohm Service
64
Shutting down and Recommissioning
65
Capillary Connections
66
Door
66
Handling the Eluent
66
Manufacturing Eluent
66
Changing the Eluent
67
Notes on Operating the High-Pressure Pump
67
Servicing the High-Pressure Pump
68
Figure 18 High-Pressure Pump - Parts
68
Figure 19 High-Pressure Pump - Cross-Section
75
Figure 20 Tool for Piston Seal (6.2617.010)
75
Figure 21 Removing the Piston Cartridge from the Pump Head
76
Figure 22 Inserting the Piston Seal into the Tool
77
Figure 23 Parts of the Piston Cartridge
78
Servicing the Inline Filter
81
Figure 24 Inline Filter - Removing the Filter
82
Servicing the Pulsation Absorber
84
Injection Valve
84
Suppressor
84
Notes for Operating the Suppressor
84
Taking Care of the Suppressor Housing
85
Servicing the Suppressor
85
Figure 25 Parts of the Suppressor
85
Peristaltic Pump
92
Notes on Operating the Peristaltic Pump
92
Servicing the Peristaltic Pump
92
Figure 26 Pump Tubing Connection - Replacing the Filter
93
Servicing the Detector
94
Rinsing the Sample Path
94
Separation Column
95
Separating Efficiency
95
Protecting the Separation Column
96
Storing the Separation Column
96
Regenerating the Separation Column
96
5 Troubleshooting
97
6 Technical Specifications
101
Reference Conditions
101
Instrument
101
Ambient Conditions
101
Housing
102
Injection Valve
102
Suppressor
102
Peristaltic Pump
103
Detector
103
Power Connection
103
Interfaces
103
Weight
104
7 Accessories
105
Index
106
5
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Metrohm 883 Basic IC plus Specifications
General
Brand
Metrohm
Model
883 Basic IC plus
Category
Laboratory Equipment
Language
English
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