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PDA-7000
Shimadzu PDA-7000 User Manual
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5
Maintenan
ce
5-
16
25
Ti
ghten
the
lock
nut
and
f
ix
the
electrode po
sition.
26
Place
an
analytical
sa
m
ple
on
the
spar
k
st
and
and
tighten
the
BYP
ASS
needle
valve
to
ret
urn
the
argon
gas
flow rate t
o the origina
l BYP
ASS rate.
27
Turn
on
the
SOURCE
switch
on
the
switch
panel
and
turn
on
the
power
of
the
excitat
ion unit.
79
81
Table of Contents
Introduction
3
Indications Used in this Manual
5
Warning Labels
6
Safety Instructions
7
Installation Site
7
Installation
7
Operation
8
In an Emergency
10
During a Power Outage
10
Handling High-Pressure Gas
11
Warranty
13
After-Sales Service and Availability of Replacement Parts
14
Disposal Precautions
15
Table of Contents
16
Definition of Terminology
20
Parts List
21
Checking of Parts
21
Consumables and Maintenance Parts
22
Repair Parts
23
How to Distinguish Similar Parts
24
Configuration and Function of the Instrument
25
Switch Panel
27
Spark Stand
29
Spectrometer
31
Condenser Lens
31
Temperature Control Circuit
31
Lamp
32
Evacuation System
32
Read-Out Unit
33
Photo Detector (PMT)
33
Photo Detector Sensitivity Controller (Attenuator)
33
Integrator
33
Data Processor System
34
Specification
38
Spectrometer
38
Excitation Unit
38
Spark Stand
38
Excitatiion Source Unit
38
Read-Out Unit
39
Data Processor System
39
Hardware
39
Software
40
Starting and Stopping the Instrument
43
Inspection before Using the Instrument
44
Starting the Instrument (Daily Use)
45
Starting the Instrument after It Has Not Been Used for a Long Time
46
Shutting down the Instrument (Daily Use)
47
Shutting down the Instrument for a Long Time
48
Emergency Stop and Recovering
49
Emergency Stop
49
Recovering from Emergency Stop
50
Operation
51
Argon Gas Bubbler
52
Checking Gas Flow Rate
54
When the Instrument Is in Operation
54
When the Instrument Is Not Used or at Nighttime
55
Turning on / off Photo Detector
56
Sample Pretreatment
57
Setting the Sample
59
Content Analysis
60
Recalibration
61
Master Curve Recalibration
63
Check Analysis
64
Maintenance
65
Maintenance and Inspection Items
66
Periodical Maintenance
66
Other Maintenance
66
Work Required after Maintenance Service
67
Maintenance Service by Shimadzu Service Engineer
67
Maintenance Flow
68
Maintaining the Spark Stand
69
Maintenance Cycle
70
Maintenance Procedure
72
Exchanging the Electrode O-Ring
82
Cleaning the Condenser Lens
83
Adjusting the Control Gap
87
Replacing Pump Oil
90
Manual Scanning
91
Lamp Test
93
Waste Discharge
94
File Utility
95
Saving (Backup)
95
Loading (Restoration)
96
Replacing Recalibration Samples
97
Replacing Argon Gas Cylinder
98
Periodic Inspection
98
Cleaning the Temperature Control Fan Heater
98
Installation
102
Temperature and Humidity
102
Vibration
102
Dust
102
Grounding
102
Power Supply
103
Argon Gas
103
Exhaust Equipment
103
Peripheral Equipment
104
Other Environmental Requirement
104
Moving and Disposing of the Product
104
Troubleshooting
105
Basic Items to be Checked
106
Troubleshooting
106
Installing the Software
108
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Shimadzu PDA-7000 Specifications
General
Brand
Shimadzu
Model
PDA-7000
Category
Measuring Instruments
Language
English
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