EasyManua.ls Logo

GL Sciences OPTIC-4 User Manual

GL Sciences OPTIC-4
118 pages
To Next Page IconTo Next Page
To Next Page IconTo Next Page
Page #1 background imageLoading...
Page #1 background image
OPTIC-4 Multimode GC Inlet
User’s Guide:
Installation and
Operation

Table of Contents

Question and Answer IconNeed help?

Do you have a question about the GL Sciences OPTIC-4 and is the answer not in the manual?

GL Sciences OPTIC-4 Specifications

General IconGeneral
BrandGL Sciences
ModelOPTIC-4
CategoryLaboratory Equipment
LanguageEnglish

Summary

Precautions and Warnings

Installation Precautions and Warnings

Safety guidelines for installing the OPTIC-4 in a lab environment by trained personnel, including ventilation and electrical safety.

Operation Precautions and Warnings

Safety measures during operation, including handling solvents, high temperatures, and electrical hazards.

Cryogenic Trap Precautions and Warnings

Specific safety advice for handling the cryogenic trap, including use of LN2/CO2 and avoiding contamination.

System Overview

Advanced Electronic Flow Control

Explanation of the sophisticated gas control system, including main and auxiliary flow channels.

Hardware

Flow Control System

Schematic diagram and explanation of the OPTIC-4 gas flow control system, including main and auxiliary EFC.

Cryogenic Trap Options

Description of the cryogenic trap options for solving peak tailing and band broadening issues.

Hardware Installation

Installing the Inlet

Steps for installing the OPTIC-4 inlet directly into the GC oven insulation for optimal performance.

Gas Lines Connections

Instructions for connecting carrier gas, inlet gas lines, exhaust, and cooling air using pneumatic fittings.

Inlet Cooling

Description of different cooling options for the inlet, including compressed air, CO2, and LN2.

Electrical Connections

Procedures for connecting inlet power, solvent monitor, and thermocouples.

Connection to Host PC

Connecting OPTIC-4 to a PC running Evolution Workstation software via USB or LAN.

Liner and Column Installation

Procedures for installing inlet liners and GC columns, depending on application requirements.

Cryotrap Installation

Steps for installing the cryotrap, including control board, mounting in GC oven, and connections.

Software Installation and Configuration

Installing Evolution Workstation Software

Step-by-step guide for installing the Evolution Workstation software from the CD-ROM.

Communication Parameters

Configuration of communication settings between the OPTIC-4 controller and the host PC via USB or LAN.

Configuration Parameters

Setting various system configuration parameters, including standby, system, and communication settings.

Standby Parameters

Setting system parameters to maintain during standby state, such as temperature, flow, and timeout.

System Configuration Parameters

Configuring system-wide parameters like IP address, maximum temperature, and carrier gas type.

Basic Operation

Instrument Startup and Shutdown

Step-by-step procedures for starting up and shutting down the OPTIC-4 instrument and PC.

Evolution Workstation Status View

Understanding the status view window in Evolution Workstation for monitoring system parameters and run graphs.

Defining and Running Methods

Method Types

Overview of the five predefined method types supported by OPTIC-4: Split, Splitless, LVI, LINEX, Expert.

Large Volume Injection Method

Implementing rapid large volume injection (LVI) up to 100 µl for improved detection limits.

LINEX Method

Using OPTIC-4 for automated thermal desorption of gas and solid samples with LINEX method.

Expert Method

Description of the Expert method for full control over all parameters and custom temperature/flow profiles.

Method Definition

Steps to define new methods by selecting predefined types and adjusting parameters in the software.

Method Parameters

Detailed explanation of various method parameters, including general, temperature, and flow controls.

Temperature Parameters

Setting initial, final temperatures, ramp rates, and hold times for the inlet's temperature profile.

Column Flow Parameters

Configuring carrier control mode, transfer time, and column flow/pressure settings.

Solvent Venting Parameters

Parameters for solvent venting, including vent mode, vent time, and solvent monitor thresholds.

Expert Method Parameters

Detailed settings for Expert methods, allowing up to nine segments for temperature and flow profiles.

Running Methods

Understanding the state transition diagram and how OPTIC-4 executes methods.

Running Method from Evolution Workstation

Steps to send a saved method to the OPTIC-4 unit for execution via the software.

Defining and Running Sequences

Advanced OPTIC-4 Features

Automated Solvent Vent Mode

Utilizing the built-in solvent monitor for automated solvent elimination time determination.

Cryotrap Control

Facilities for controlling the GL Sciences Cryogenic Trap for sample collection and analysis.

Operating Cryogenic Trap

Cryotrap Temperature Profile

Setting cryotrap parameters like low temperature, hold time, and heat ramp rate for optimal trapping.

Maintenance

Inlet Cleaning

Procedure for cleaning the inlet to resolve carryover or background contamination issues.

Carrier Gas Leak Check

How to perform a leak check on the carrier gas supply and connections using an electronic leak detector.

Troubleshooting and Diagnostics

Troubleshooting

Guide to identify and resolve common problems encountered during OPTIC-4 installation and operation.

Errors and Warnings

Explanation of error and warning messages displayed by the system and their potential causes.

Technical Specifications

Electronic Flow Control

Specifications for the EFC channels, pressure/flow ranges, sensors, and carrier gas compatibility.

Cryotrap Option

Specifications for the cryotrap option, including operating temperature range and cooling methods.

Appendix D: Examples of OPTIC-4 Method Profiles

D.3 Large Volume Injection method

Example method profile for large volume injection (LVI) showing parameter settings.