GL Sciences OPTIC-4

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OPTIC-4 User’s Guide

Issue 5.3

Contents

Page ix

Appendix F: Liner Selection Guide ............................................................................................. F.1

Main Page

Default Chapter6
- Table of Contents6
Precautions and Warnings11
- General Precautions11
- Installation Precautions and Warnings11
- Operation Precautions and Warnings12
- Warnings Signs14
- Cryogenic Trap Precautions and Warnings14
Waarschuwingen en Aandachtspunten16
- Algemene OPTIC-4 Waarschuwingen en Aandachtspunten16
- Algemene OPTIC-4 Waarschuwingen16
- Algemene OPTIC-4 Aandachtspunten17
- Waarschuwingen en Aandachtspunten Voor de OPTIC-4 Cryotrap17
- Waarschuwingen Voor de OPTIC-4 Cryotrap17
- Aandachtspunten Voor de OPTIC-4 Cryotrap17
Sicherheitshinweise und Warnungen18
- OPTIC-4 - Allgemeine Sicherheitshinweise und Warnungen18
- OPTIC-4 - Allgemeine Warnungen18
- OPTIC-4 - Allgemeine Warnungen19
- Sicherheitshinweise und Warnungen Betreffend die OPTIC-4 Kühlfalle19
- Warnungen Betreffend die OPTIC-4 Kühlfalle19
注意事项与警告20
- 一般注意事项与警告20
- 安装注意事项与警告20
- 操作注意事项与警告21
- 警告标识22
- 冷阱注意事项与警告23
Mises en Garde Et Précautions D'emploi25
- Mises en Garde Et Précautions D'emploi Générales Concernant OPTIC-425
- Mises en Garde Générales Concernant OPTIC-425
- Précautions D'emploi Générales Concernant OPTIC-426
- Mises en Garde Concernant Le Piège Cryogénique D'optic-426
- Précautions D'emploi Concernant Le Piège Cryogénique D'optic-426
Advertencias y Precauciones27
- Advertencias y Precauciones Generales Relacionadas con el OPTIC-427
- Advertencias Generales en Torno al OPTIC-427
- Precauciones Generales OPTIC-428
- Advertencias y Precauciones Relacionadas con el Crioseparador OPTIC-428
- Advertencias Relacionadas con el Crioseparador del OPTIC-428
- Precauciones Relacionadas con el Crioseparador del OPTIC-428
Avvertenze E Precauzioni29
- Avvertenze E Precauzioni Generali Dell' OPTIC-429
- Avvertenze Generali Dell' OPTIC-429
- Precauzioni Generali Dell' OPTIC-430
- Avvertenze E Precauzioni Relative al Cryotrap Dell'optic-430
- Avvertenze Relative al Cryotrap Dell'optic-430
- Precauzioni Relative All'optic-4 Cryotrap30
System Overview31
- High Performance31
- Advanced Electronic Flow Control31
- Improved Flexibility32
- Compatibility32
Hardware33
- Control Unit33
- Keypad33
- Status Led's34
- Rear Panel35
- Flow Control System37
- Inlet Hardware37
- OPTIC-4 Local Control39
- OPTIC-4 Keypad39
- Status Led's39
- PC Control40
- Cryogenic Trap Options40
- Cryotrap Hardware40
- Trap Rear Panel Connections40
- Auxiliary EFC Unit40
- Master/Slave Mode40
Hardware Installation42
- Installing the Inlet42
- Inlet Location42
- Inlet Installation43
- Gas Lines Connections43
- Carrier Gas Line44
- Inlet Gas Lines44
- External Solvent Monitor45
- Exhaust and SP Exhaust Ports46
- Inlet Cooling46
- Electrical Connections47
- Inlet Power Connection47
- External Equipment48
- Connection to Host PC48
- Liner and Column Installation48
- Liner Installation48
- Column Installation48
- Cryotrap Installation50
- Installation of Cryotrap Control Board50
- Installation of Cryotrap into GC Oven50
- GC Column Installation53
- Cryotrap Electrical Connections55
Software Installation and Configuration56
- Introduction56
- PC Requirements56
- Installing Evolution Workstation Software56
- Communication Parameters57
- USB Communication57
- LAN Communication59
- Configuration Parameters60
- Standby Parameters60
- System Configuration Parameters62
- OPTIC-4 User's Guide Issue62
- External Communication65
- Access Control66
- Calibration Parameters (Locked)66
Basic Operation67
- Instrument Parameters67
- Instrument Startup and Shutdown67
- Evolution Workstation Status View68
Defining and Running Methods69
- Introduction69
- Method Types69
- Split Methods69
- Splitless Methods69
- Large Volume Injection Method69
- Expert Method71
- Method Definition71
- Method Parameters73
- General Method Parameters73
- Temperature Parameters73
- Column Flow Parameters74
- Solvent Venting Parameters75
- Split Flow Parameters75
- Auxiliary Outputs76
- Expert Method Parameters76
- Running Methods78
- Running Method from Evolution Workstation79
- Stopping Method from Evolution Workstation79
- Optimizing Method79
- Converting Method to an Expert Method79
Defining and Running Sequences81
- Defining Sequences Using Evolution Workstation Software81
- Running Sequences Using Evolution Workstation Software81
Advanced OPTIC-4 Features82
- Automated Solvent Vent Mode82
- Solvent Cooling Effect83
- Floating Final Temperature83
- Negative Temperature Ramps in Expert Method84
- Cooling Valve Mode84
- Auxiliary Outputs84
- Cryotrap Control84
- Technical Notes85
Operating Cryogenic Trap86
- Configuring Cryotrap86
- Cryotrap Temperature Profile86
Maintenance88
- Routine Maintenance88
- Inlet Cleaning88
- Carrier Gas Leak Check89
- Servicing91
Troubleshooting and Diagnostics92
- Troubleshooting92
- Instrument Does Not Power up92
- Inlet Does Not Heat up92
- Inlet Heats up Slowly92
- Inlet Cools down Slowly93
- Flow/Pressure Set Point Can Not be Reached93
- Errors and Warnings93
- Inlet Thermocouple Fault93
- Inlet Earth Fault94
- Inlet Overpower94
- Inlet Temperature above Maximum94
- Cryotrap Thermocouple Fault94
- Cryotrap Earth Fault94
- Cryotrap Overpower94
- Cryotrap Temperature above Maximum95
- Inlet Temperature Warning95
- Cryotrap Temperature Warning95
- Inlet Pressure Warning95
- Auxiliary Flow Warning96
Technical Specifications97
Appendix A: OPTIC-4 Default Configuration Parameters99
- Standby Parameters99
- System Configuration Parameters99
Appendix B: Rear Panel I/O Connections101
- Gas Chromatograph Interface101
- Auxiliary Outputs102
Appendix C: Accessories, Consumables, and Spares103
- Accessories/Upgrades104
- Installation Kits104
- C.5 Accessories/Upgrades104
Appendix D: Examples of OPTIC-4 Method Profiles105
- Split Method105
- Splitless Method106
- D.2 Splitless Method106
- Large Volume Injection Method107
- Expert Method109
- D.5 Expert Method109
Appendix E: Cryogenic Trap Cooling Line Diagrams110
- Liner Selection Guide112

GL Sciences OPTIC-4 - Page 10

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