8.14
Appendices
Pinnacle Operators Manual
Pickering Laboratories Inc.
Threonine Peak Area
Average Peak
Area
Standard
Deviation
% CV Specification Pass / Fail
Run 1
Run 2
Run 3 ≤ 1.5%
Run 4
Run 5
Run 6
Serine Peak Area
Average Peak
Area
Standard
Deviation
% CV Specification Pass / Fail
Run 1
Run 2
Run 3
≤ 1.5%
Run 4
Run 5
Run 6
Cysteic Acid Peak Area
Average Peak
Area
Standard
Deviation
% CV Specification Pass / Fail
Run 1
Run 2
Run 3
≤ 1.5%
Run 4
Run 5
Run 6
Method Table
Time Buffer A* RG003
0 100 0 Column Temp: Refer to column insert.
20 100 0 Eluant Flow Rate: Refer to column insert.
20.1 0 100 Reactor Temperature: 130 deg C
24 0 100 Reagent Flow Rate: 0.3mL/min
24.1 100 0
Stop Time 24 min
Post Time 12 min
* Use the A Buffer corresponding to the column you have. The column insert will have
the correct initial buffer listed in the method.
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