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General| Category | Analytical Instruments |
|---|---|
| Temperature Control | Ambient to 60°C |
| Type | Post-column derivatization system |
| Power Requirements | 100-240 VAC, 50/60 Hz |
| Detector | Not specified (compatible with fluorescence and UV detectors) |
| Pump Type | Dual piston |
| Injection Volume | N/A (post-column system) |
| Flow Rate Range | 0.001 to 5.0 mL/min |
Guide on how to navigate and utilize the Pinnacle PCX operator manual effectively.
Essential preliminary information and checks before operating the Pinnacle PCX instrument.
Detailed technical specifications for the Pinnacle PCX instrument and its components.
Environmental and infrastructure requirements for installing and operating the Pinnacle PCX.
Explanation of the post-column derivatization technique and its benefits in HPLC analysis.
Key factors and considerations for developing effective post-column analytical methods.
Simplified overview of a standard HPLC system design and its components.
Principles and considerations for designing effective post-column HPLC systems.
Specific design features and innovations of the Pinnacle PCX post-column system.
Overview of the Pinnacle PCX instrument's components, layout, and basic functions.
Description and function of the column check valve in the Pinnacle PCX.
Details on connecting columns and the operation of the column oven.
Explanation of the syringe-type reagent pump used in the Pinnacle PCX.
Description of the reagent valve's function and operating positions.
Information on the reagent, wash, and flush bottles and their placement.
Overview of the fluidics panel, its components, and layout.
Details on the PTFE capillary reactor and its replacement.
Information on connecting the detector to the Pinnacle PCX system.
Description of the pump compartment containing reagent pumps and gas manifold.
Details on the gas manifold for pressurizing reagent reservoirs.
Explanation of the display module and its controls for monitoring the instrument.
Description of the electronics compartment housing the main PC board and power supply.
Overview of the communication ports and power connections on the back panel.
Key safety features designed to protect the instrument and user from hazards.
Description of available standard configurations for the Pinnacle PCX instrument.
Detailed site requirements including bench space, electrical, and gas supply.
Procedure for unpacking and preparing the Pinnacle PCX for installation.
Instructions for connecting the gas supply to the back panel of the Pinnacle PCX.
Guidelines for connecting the Pinnacle PCX to a computer via USB or network.
Steps for installing the Pinnacle PCX control software on the computer.
Procedure for connecting the HPLC pumps and autosampler to the Pinnacle PCX.
Steps for priming the eluant lines and system components.
Instructions for installing the analytical and guard columns.
Guidance on connecting the HPLC detector to the post-column system.
Procedure for connecting the reagent reservoirs to the system.
Steps for preparing the reagent pumps for operation.
Procedure for setting up and running the first chromatogram.
Procedures for properly shutting down the Pinnacle PCX system.
Introduction to the Pinnacle PCX control software and its capabilities.
Description of the status window, its icons, and displayed information.
Overview of the menu options available in the Pinnacle PCX software.
Steps for configuring the Pinnacle PCX settings via the software interface.
Explanation of how to collect and use log files for troubleshooting.
Guide to creating, editing, saving, and deleting post-column analysis methods.
Procedure for creating, editing, and managing analysis sequences.
Step-by-step tutorials for creating methods and sequences.
Detailed steps for starting and running a post-column analysis.
Procedure for stopping and resetting the instrument in case of emergency.
Methods for safely shutting down the Pinnacle PCX system.
Recommendations for maintaining the Pinnacle PCX for optimal performance.
Helpful suggestions and practices for operating the Pinnacle PCX.
Detailed procedures for properly shutting down the system to prevent damage.
General procedures for cleaning and maintaining key instrument components.
Instructions for replacing the reagent filters in the Pinnacle PCX.
Procedure for replacing the ambient reactor in the system.
Steps for replacing the heated reactor cartridge.
Procedures for maintaining and servicing the instrument valves.
Detailed guide for replacing the pump seals to maintain system integrity.
Instructions for safely replacing the instrument's fuses.
Diagrams and information related to tubing kits for the Pinnacle PCX.
Detailed application guide for amino acid analysis using the Pinnacle PCX.
Application guide for carbamate analysis, including sample prep and conditions.
Application guide for glyphosate analysis, covering sample prep and conditions.
Contact information and methods for obtaining technical support.
Importance and use of the instrument parameter log for troubleshooting.
General advice and rules for effective troubleshooting of instrument issues.
Identification and solutions for common system-level problems.
Troubleshooting guides for common chromatography issues like baseline and noise.
Common issues related to columns and their resolution.
Troubleshooting specific to Amino Acids, Carbamates, and Glyphosate analyses.
Common software-related issues and their troubleshooting steps.
Specific procedures for resolving common system and column issues.
Procedure for qualifying the installation and operation of the Pinnacle PCX.
Checklist for verifying installation and operational qualifications.
Data sheet for recording performance qualification results like flow rate and temperature.
Template for logging instrument parameters at initial conditions.
Schematic flow diagrams for simplex and duplex configurations.
List of recommended consumables and spare parts for the Pinnacle PCX.
Information regarding the warranty coverage for instruments and columns.
List of cited literature and resources for further information.
