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Shimadzu GCMS-QP2010 - Page 139

Shimadzu GCMS-QP2010
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ZEAV-0416A
Shimadzu Corporation
2010 Installation Completion Checklist
The items relate to acquiring installation completion data and conducting operation checks.
Installation is complete when all items in the installation completion checklist have been checked and
the operation instruction completed. (A standard installation requires four working days.)
Analysis of the customer's samples is separate from the installation process.
Checklist
No. Check Item Check Details and Conditions Criteria Check Comment
1
Installation
conditions
Power supply:120/ 220/230/240V
Check supply capacity (see System User
Guide)
Grounding (100 max.)
Location:
Space designated in System User Guide
available?
Check strength of table (able to support
100kg?)
Temperature:
Check ambient conditions at installed
location.
Gas (Helium purity and pressure regulator)
He purity
Designated pressure and contamination
check
Exhaust:
Is RP exhaust outlet connected to exhaust
outside the building or is an oil-mist filter
used?
within ±5%
Greater than indicated value.
Grounded
Available
No flexing or vibrations
within 23±5
M
C
99.995% min.
No abnormality in analysis
data
Yes
( V)
( A)
2
Operation checks
a. Basic operation
b. Explanation
* Do the RP/TMP start normally with the
GCMSsolution startup program? (Automatic
start completes within 5 minutes?)
* Normal communication with GC using the
GCMSsolution GC parameters?
* Temperature control of INJ, OVEN, I/F units?
* Explain MS, MC, and SIM measurement using
OFN 100pg/µL standard sample (tuning,
creating methods, analysis, batch processing,
data re-analysis, outputting reports).
Normal
Normal
READY lamp does not go
out
Operation explained
3
Function checks
a. Tuning
* Peak intensity fluctuates when each lens
voltage is changed in the tuning window.
* Detector voltage stabilizes at -1.8kV or below
after auto-tuning? (This checks the ion-source
operation, SI sample injected volume, and
detector performance.)
* Discrepancy in peak amplitudes within 0.1M
after auto-tuning?
* When pattern correction is selected
m/z502 intensity over 2% of m/z69 intensity?
Keep auto-tuning data.
Fluctuates
-1.8kV or below
Within 0.1M
Over 2%

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