ZEAV-0416A
Measure S/N.(EI MODE and NCI MODE)
EI SAMPLE OFN 1pg/ul (isookutane solvent) 1ul m/z272 S/N≧60
NCI SAMPLE OFN 0.1pg/ul(100fg/ul)( isookutane solvent) 1ul m/z272 S/N≧100
Measurement Conditions
INJ 250
M
C
SPLITLESS mode (sampling time 1.0 minute)
COL: 50
M
C (1min) - 40
M
C / min - 200
M
C (0min) - 15
M
C / min - 280
M
C
I/F: 250
M
C
IS: 200
M
C
He: during injection 250kPa, 1 minute (HIGH-PRESSURE INJECTION mode)
during analysis 120Kpa
Total flow: 50mL/minute
MS: SCAN mode (mass range: m/z200 to 300)
interval 0.5s
detector voltage relative value: +0.4 (absolute value: 1.4 to 1.6kV)
measurement time: 3.0 to 10.0 minutes (solvent elution time: 3 minutes)
Measure S/N.(CI MODE)
Benzophenone 100pg/ul (acetone solvent) 1ul m/z183 S/N≧150
Measurement Conditions
INJ: 250℃SPLITLESS MODE (Sampling Time 2.0 min)
COL: 80℃(2min)−30℃/min−260℃(5min)
I/F: 250℃IS:200℃
He:
during injection and analysis 100Kpa
Total flow 20ml/min
MS: SCAN MODE (mass range M/Z 100〜250)
interval 0.5sec
detector voltage
relative value +0.4 (absolute 1.4〜1.6 kV)
measurement time6.0〜11.0 min (solvent elution time 5.5min)
Reference pressure of the reagent gas in the installation at the time of corporate identity, NCI use
Methane gas CI 100Kpa〜300Kpa NCI 200Kpa〜300Kpa
Isobutane gas CI 20Kpa〜80Kpa NCI 40Kpa〜80Kpa
Ammonia gas CI 100Kpa〜300Kpa NCI 200Kpa〜300Kpa
mass patern check Measurements DI MODE
Carry out temperature adjustment on the set-up temperature
cholestane 100ng/ul (acetone solvent) 1ul
Measurement Conditions
MS I/F 100℃
IS 250℃
DI temperature room temperature to 300℃ 40
M
C / min
GC temperature constant
Colum flow moderate flow