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Shimadzu GCMS-QP2010 User Manual

Shimadzu GCMS-QP2010
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ZEAV-0416A
Measure S/N.(EI MODE and NCI MODE)
EI SAMPLE OFN 1pg/ul (isookutane solvent) 1ul m/z272 S/N60
NCI SAMPLE OFN 0.1pg/ul(100fg/ul)( isookutane solvent) 1ul m/z272 S/N100
Measurement Conditions
INJ 250
M
C
SPLITLESS mode (sampling time 1.0 minute)
COL: 50
M
C (1min) - 40
M
C / min - 200
M
C (0min) - 15
M
C / min - 280
M
C
I/F: 250
M
C
IS: 200
M
C
He: during injection 250kPa, 1 minute (HIGH-PRESSURE INJECTION mode)
during analysis 120Kpa
Total flow: 50mL/minute
MS: SCAN mode (mass range: m/z200 to 300)
interval 0.5s
detector voltage relative value: +0.4 (absolute value: 1.4 to 1.6kV)
measurement time: 3.0 to 10.0 minutes (solvent elution time: 3 minutes)
Measure S/N.(CI MODE)
Benzophenone 100pg/ul (acetone solvent) 1ul m/z183 S/N150
Measurement Conditions
INJ 250SPLITLESS MODE (Sampling Time 2.0 min)
COL: 80℃(2min)−30℃/min260℃(5min
IF: 250IS200℃
He:
during injection and analysis 100Kpa
Total flow 20ml/min
MS: SCAN MODE mass range M/Z 100250
interval 0.5sec
 detector voltage
relative value +0.4 absolute 1.41.6 kV

measurement time6.011.0 min solvent elution time 5.5min
Reference pressure of the reagent gas in the installation at the time of corporate identity, NCI use
Methane gas CI 100Kpa300Kpa NCI 200Kpa300Kpa
Isobutane gas CI 20Kpa80Kpa NCI 40Kpa80Kpa
Ammonia gas CI 100Kpa300Kpa NCI 200Kpa300Kpa
mass patern check Measurements DI MODE
Carry out temperature adjustment on the set-up temperature
cholestane 100ng/ul (acetone solvent) 1ul
Measurement Conditions
MS I/F 100
IS 250
DI temperature room temperature to 300 40
M
C / min
GC temperature constant
Colum flow moderate flow

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Shimadzu GCMS-QP2010 Specifications

General IconGeneral
BrandShimadzu
ModelGCMS-QP2010
CategoryLaboratory Equipment
LanguageEnglish

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