Agilent Technologies 5100 Service Manual

260 Agilent Restricted Agilent 5110/5100 ICP-OES Service Manual
9 iTroubleshoot/Parts Predict
Problem Solving Table
Low Intensities Low Intensities at high/Low
Wavelengths (May not
Calibrate)
Sample Intro blockage Tubing kinked, blocked, dirty -
Rectify
2410020500
Low Intensities Low Intensities at high/Low
Wavelengths (May not
Calibrate)
Sample Intro blockage Torch injector blocked - Clean G8010-60228
Low Intensities Low Intensities at high/Low
Wavelengths (May not
Calibrate)
Wavelengths Off Peak Recalibrate Instrument
Low Intensities Low Intensities at high/Low
Wavelengths (May not
Calibrate)
Wrong Std Concentration Prepare new standards 6610030100
Low Intensities Low Intensities at Low
Wavelengths (May not
Calibrate)
Blocked Purge Filter Replace Purge Filter G8010-60136
Low Intensities Low Intensities at Low
Wavelengths (May not
Calibrate)
Purge time insufficient Purge for 4 hrs minimum and
ensure all purges are on
Low Intensities Low Intensities at Low
Wavelengths (May not
Calibrate)
Windows Contaminated Replace Axial/Radial Windows G8010-68014,
G8010-68015
Low Intensities No Signal Spraychamber not misting No Nebulizer gas due to fitting
not pushed home - Reseat
Low Intensities No Signal Spraychamber not misting Nebulizer Blocked - Clean or
replace
G8010-60255
Low Intensities No Signal Spraychamber not misting No uptake due to wrong pump
pressure - adjust
Low Intensities No Signal Spraychamber not misting Pump tubes stretched - Replace
Low Intensities Random Wavelengths
intensities failing
Contaminated Blank Prepare new blank 5190-7001
Low Intensities Random Wavelengths
intensities failing
High Dark Current values Recalibrate Detector - Check for
light leak, shutter sticking
Low Intensities Random Wavelengths
intensities failing
High Dark Current values Realign Optics, Check Camera
offsets using PolyAlign S/W
Low Intensities Random Wavelengths
intensities failing
Moisture on Detector Lens Moisture in purge gas supply
(Argon) - Switch off chiller for
30mins to verify. Check with
Polyalign/LED on, no plasma
and 10ms integrate. There
should be no peaks, especially,
in the region 330-180nm (DLA
43 to 35)
Low Intensities Random Wavelengths
intensities failing
Sample Matrix issue Interference from EIE's. Change
to Radial view
Low Intensities Random Wavelengths
intensities failing
Wavelengths Off Peak Recalibrate Instrument
Low Intensities Random Wavelengths
intensities failing
Wavelengths Off Peak Allow 4 hours for instrument
warmup
Low Intensities Air Present in optics Ensure Purging is on Optics Purge, Boost Purge, Cone
Purge, Snout Purge all on
Table 1
Symptom Area Problem Problem Description Solution Part Number(s)

Agilent Technologies 5100 Specifications

General

Brand	Agilent Technologies
Model	5100
Category	Laboratory Equipment
Language	English