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HP 5973 - To Install a Capillary Column Using the Installation Tool

HP 5973
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28
1 Installing GC Columns
To install a capillary column using the installation tool
To install a capillary column using the installation tool
Materials needed:
Column cutter (5181-8836)
Column installation tool (G1099-20030)
Ferrules
0.3-mm id, for 0.10-mm id columns (5062-3507)
0.4-mm id, for 0.20- and 0.25-mm id columns (5062-3508)
0.5-mm id, for 0.32-mm id columns (5062-3506)
0.8-mm id, for 0.53-mm id columns (5062-3538)
Gloves, clean
large (8650-0030)
small (8650-0029)
Interface column nut (05988-20066)
Septum (may be old, used inlet septum)
Wrenches, open-end, 1/4-inch × 5/16-inch (8710-0510) – 2 required
For optimal sensitivity performance, see To install a capillary column without
the installation tool, 26.
1 Slide a septum, interface column nut, and conditioned ferrule onto the
free end of the column.
The tapered end of the ferrule should point toward the nut.
2 Insert the column into the column installation tool.
Slide the column through until the end extends past the end of the tool.
3 Cut 1 cm off the end of the column (page 20).
4 Position the column so that 1 to 2 mm extends past the end of the tool.
Hand tighten the nut.
5 Slide the septum to touch the end of the nut.
The septum will help assure that the position is correct.
6 Use two wrenches to tighten the nut 1/4 turn.
The column should not slide when tugged gently.
7 Remove the column and nut from the installation tool.
The total length from the septum to the end of the column is 176 mm.

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