Pickering Laboratories Pinnacle PCX - Page 119

6.3-6
Section 6
ApplicAtions
Pinnacle Operators Manual
Pickering Laboratories Inc.
METHOD 1: 0840250 C
8
COLUMN (4.0X250MM) WATER/METHANOL GRADIENT WITH METHANOLIC AND
AQUEOUS SAMPLES
HPLC FLOW RATE: 0.8ML/MIN COLUMN TEMPERATURE: 50˚ C REAGENT FLOW RATE: 0.3ML/MIN
CONDITIONS FOR WATER/METHANOL GRADIENT
Time (Min) Water % MeOH %
0 85 15
2 85 15
42 30 70
46 30 70
46.1 0 100
51 0 100
51.1 85 15
59 85 15
Carbamate Test Mix, 2.5ppm, 10ul injection, 25cm, Carbamate C
8
column (0840250)
Carbamate Test Mix, 0.25ppb, 100ul injection, 25cm, Carbamate C
8
column (0840250)
1
2
3
4
5
6
7
8
9
N
11
10
0
10
20
30
40
min
1
2
3
4
5
6
7
8
9
N
11
10
0
10
20
30
40
min